Tests were conducted on 6 samples for each soil type where multiple samples for each soil type can be seen in
Figure 1. However, we were unable to observe the cracking behaviors on all of the tests using an infrared camera due to the following three conditions: (a) cracks occurred on the backsides of the samples, (b) samples disintegrated without cracking due to melting (see
Figure 4a,b), and (c) samples yielded without cracking (see
Figure 4c). Cracking occurred on either one or both sides of the specimen by chance, which cannot be practically controlled. Yielding and disintegrating of specimens occurred as the specimens were partially melted. The authors indeed attempted to repeat the tests under a lower room temperature (around 15 °C) in the winter, however, satisfactory improvements on avoiding the melting of specimens were not achieved. To avoid the melting of specimens, the compression tests on specimens should be conducted under temperatures below the freezing point of water [
19,
20,
21]. In the previous research [
19,
20,
21], the low temperature of specimens during testing was maintained by immersing the specimens in liquid cool materials. Unfortunately, such cooling systems were not available to the authors and restricted the direct observation of specimens using the infrared thermographic camera during compression tests. Therefore, specimens were not guaranteed to be completely frozen during our tests. One sample of each soil type was analyzed as they demonstrated evident cracking behavior.
Due to a lack of pre-existing knowledge of conditions under which a crack would appear in thermograph of frozen soils, the thermographs were carefully examined frame by frame. The qualification of a crack can be qualitatively described as follows:
According to the above description, two types of curves are plotted to demonstrate the temperature change at a crack point. The T-t curve shows how the temperature at the crack point varies temporally. The T-d curve shows how the temperature at the crack point varies spatially. Moreover, the load-time curve is used to qualitatively determine the strain-stress status of the specimen. It was assumed that the frozen soil specimens displayed elastic-plastic behavior. The period before the load peaks is defined as the elastic stage and the period after as the plastic stage. To convert the unit of distance measured in the thermograph from pixel to mm, the thickness of the lower platen of the compression machine was used to calculate the conversion ratio from pixel to mm. The calculated conversion ratios for frozen clay, sand and gravel were 0.60, 0.62, and 0.65 mm/pixel, respectively.
3.1. Crack in Frozen Clay
As shown in the load-time curve in
Figure 5, the load peaked at 96.30 s after the test commenced. After 96.30 s, the temperature of certain points on the specimen’s surface appears to increase at a slightly higher rate than the rest. One example is indicated in
Figure 6 as the crack point. A baseline point about 4 mm downwards of the crack point was selected to mitigate the effect of measurement errors and the effect of heating from the ambient atmosphere on the variation of temperature. The
(temperature change)-t (time) curve for the crack point and baseline points are plotted in
Figure 7. The temperature profile was set relative to temperature changes, with 0 chosen as the initial temperature at the reference point. The temperature changes were filtered by implementation of a Savitzky–Golay filter.
Disregarding the random flocculation, from 105 s to 123 s, the temperature increases from −3.02 °C to −2.41 °C.
The temperature increase at the crack point was further verified by the temperature profile along a line approximately perpendicular to the crack as shown in
Figure 8. The temperature profile at the start of the test (0 s), immediately before the crack occurs (105 s), and after the crack forms (125 s), are plotted. Before the crack occurs, there is no significant difference in temperature between the potential crack point and the rest. After the crack is formed, the temperature at the crack point is 0.57 °C higher than those at the points not influenced by the crack.
3.2. Bulge Effect in Frozen Sand
Although there was no individual crack observed in the sand case, as the frozen sand specimen was compressed, the expansion in the radial direction, which we termed bulge, became significantly visible after yield and the observation can also be correlated to temperature variations. The temperature of three representative points located at the upper part (U.), lower left part (L.L), lower right part (L.R), and the average temperature of a square area (S.) were selected to demonstrate the effect of the bulge on temperature. The locations are indicated in
Figure 9. In
Figure 9, temperatures are mostly above 0 °C as the surface of the specimen was covered by water instead of ice. The ambient air temperature was around 30 °C. The ice on the top of the specimen melted immediately after contact between the specimen and upper platen of the compression machine. Due to gravitational effects, the water subsequently ran off downwards onto the specimen surface. Although the specimen was completely frozen initially, certain parts melted during the compression test. The same observation was made for the clay specimen and gravel specimen.
The temperature and load curves are plotted together in
Figure 10. As the bulge of the specimen becomes evident after yield (64.9 s), the temperature of each single point of the specimen surface demonstrated 4 simultaneous impulsive increases initiating at 66.80 s, 88.30 s, 99.53 s, and 110.30 s, respectively. Impulses were not observed at points outside of the specimen surface, which signifies these impulses were not measurement errors. The magnitude of
for the impulses ranged from 0.37 to 0.95 °C.
3.3. Cracks in Frozen Gravel
Two types of cracks were observed during the compression test of the gravel specimen. The cracks, which occurred in-between gravel particles, caused increases of temperature at the crack point. Such cracks were denoted as I1, I2 I3, and I4 for ‘increase’. Temperature decreases at the crack point were observed for cracks which occurred within the ice block. Such cracks were denoted as D1, D2, D3, D4, D5, and D6 following the capitalized initial of the word ‘decrease’. The ideal temperature variation for cracks of types I (increase) and D (decrease) are illustrated in
Figure 11. When cracks occur between gravel particles, the inter-particle friction generates heat. However, those frictional forces were relatively negligible between ice surfaces due to their smoothness. Although there was heat generated around ice particles, the heat would probably be consumed by the melting of ice as opposed to an increase in temperature. The temperature decrease is due to a temperature gradient travelling from the surface to the inner core of the specimen. As the crack widens, the inner surface of the specimen, the temperature of which is lower compared to the outside, is exposed to the camera. The location of these two types of cracks is indicated in
Figure 12.
Temporal variations for cracks I1, D2 and D5 are shown in
Figure 13a,
Figure 13b and
Figure 13c, respectively. Crack I1 occurs at the time of yield. Before the crack initiates, the temperature of the crack point is relatively constant and approximately equal to the baseline temperature. The
-t curve of the crack point deviates from that of the baseline since t = 126.33 s. From t = 126.33 to t = 128.80 s, the temperature at the crack point increases by 0.6 °C while that at the baseline remains relatively stable. After the crack is formed, the temperature at the crack remains relatively steady from 128.90 to 135.33 s but subsequently decreases due to the decrease in load, as shown in
Figure 14.
Crack D2 forms at the transitional point between stress softening and plastic deformation, which takes less time than the formation of crack I1. This is compatible with the explanation that there is minimal friction and ice is extremely brittle The magnitude of the temperature decrease is less important than the temperature increase for the crack between gravel particles as the decrease only demonstrates the depth of the crack that develops into the specimen. Crack I5 occurs along the global failure surface during plastic deformation. The crack occurred at 265 s with a temperature increase of 0.51 °C. Following the relative movement between two parts of the specimen on each side of the failure, the surface starts at a 280 s to display a temperature increase that takes 3 steps, which corresponds to the steps of relative movement along the failure surface observed in the video. The load, and hence the stress within the specimen, is less than those observed previously during the elastic stage when I1 occurs. However, the relative movement along the global failure surface is more intense. Thus, both the rate of increase and the total amount of increase in temperature is larger. From the 280 s to 315 s, the temperature increase due to friction along the global failure surface is 2.66 °C. The spatial temperature distribution across I1, D2, and I5 are also plotted to demonstrate the increase during the formation of the crack in
Figure 15.
is defined as
where
is the temperature at crack I1 at formation and
is the average at the immediate surrounding area of crack I1.
In the same manner, the time, , represents when the crack is fully developed and is recorded for cracks I2, I3, I5, D1, D3, D4, and D6. After a crack has formed, the temperature may still vary, subject to the change in stress-strain conditions. Thus, the for crack I1 at the stress-softening stage (denoted by the initial ‘s’ as subscript in ) and plastic stage (denoted by the initial ‘p’ as subscript in ) and for Crack I2 at the plastic stage were also calculated.
The series of
,
) are plotted together with the load-time curve in
Figure 16. During the elastic stage, only two cracks, I1 and D1, occur slightly before yield (128.9 s). As the load decreases during the stress-softening period, the
at crack I1 also decreases. A series of cracks consisting of 4 types D and 1 type I occur immediately before the transition to plastic deformation at 162.0 s. Afterward, the load remains relatively constant as the compression reaches its plastic stage and no crack occurs until t = 265 s when the cracks later form the initiating global failure line. From t = 265 s to t 300 s, the global failure surface gradually grows by connecting the individual cracks and the temperature along with it generally increases. The total increase in temperature at these series of cracks are all above 2.1 °C.
Figure 17 shows the temperature profile and normalized temperature profile around I1 at yield, stress softening and failure.
is a result of frictional heat but its magnitude also depends on the thermal properties. It is assumed that the thermal properties and conditions of crack I1 remain constant during the test.
For the crack I1, values and C can be assumed constant during the test. Although the stress at the crack was not measured, it can be inferred that the stress is proportional to the load. Before the plastic stage, the deformation of the entire specimen was relatively uniform and there was little inter-particle movement. There, the is mostly determined by the load. The load is the highest at yield and subsequently decreases during the stress-softening stage while the rate of displacement shows no significant change throughout the period. Thus, is higher than . After the plastic stage was reached, although the stress is lower than before, the rate of displacement is significantly higher. The continues increasing and, when the specimen eventually fails, is much higher than and .
With the normalized profile, the propagation of frictional heat can be examined. The dimension affected by the frictional heat expands during the test but is ultimately limited by the dimensions of the gravel particle directly subjected to frictional forces. It seems the temperature of ice within the void of particles remains unaffected by the frictional heat. There are two possible explanations:
3.4. Comparison of Behavior of Plastic Stage
In
Figure 18 the spatial temperature profile of cracks from all 3 cases are plotted together. The maximum value of
is observed in
Figure 17 also plotted together with the load curve in
Figure 19a. The strain is estimated from the deformation of specimen in the videos. However, the magnitude of
cannot provide an undistorted view of the magnitude of friction as the
also depends on thermal parameters such as the specific heat capacity besides the frictional heat. Thus, the frictional heat is back-calculated from
.
A body of unit amount of mass is considered for each specimen and the body is assumed as an isolated system. Regarding the clay and gravel specimens, the body is located in the pixel referred to as the crack point. For the sand specimen, the body is located in an arbitrary position within rectangle S. Thus, the amount of frictional heat that occurred in those bodies of unit weight can be calculated as:
where
is the specific heat capacity of unit mass,
is the temporal temperature change resulting from crack or bulge. The value of
is obtained from the literature as shown in
Table 2.
As the spatial resolution was about 0.4mm/pixel in this study, for the calculation of the gravel specimen, pixels of the crack point observed were within the gravel particle, thus the
for dry gravel was directly used. For the clay and sand specimens, the
for the soil–water mixture should be used. The
for sand is very much dependent on the void ratio of the sand specimen. The
for the sand–ice mixture is assumed to be the weighted average of specific heat capacity for ice and dry sand and calculated as
where
is the specific heat capacity per unit mass of sand,
is the specific heat capacity per unit of ice,
and
are the mass of sand and ice(water) constituting the specimen,
is cited in
Table 2,
g and
are measured when the specimens are prepared.
is estimated according to an empirical equation proposed by Dickinson and Osborne [
24] as follows:
The value of T (temperature) should be assigned to the unit of K. To be consistent with the heat capacity for gravel and clay measured at 0 °C, T = 273.15 K is used in Equation (4),
2.116 J/(
). With all the values on the right-hand side in Equation (3) obtained,
can be calculated. The values of
adopted for all three cases are listed in
Table 3 and these values were used in Equation (4) to calculate the
for each case.
Figure 19b shows the
in unit mass resulting from inter-particle friction and load–strain curve for all 3 cases altogether. As shown in
Table 3, the equivalent unit weight specific heat capacity
of frozen gravel is the lowest among the three different specimens. It is assumed the frictional heat generated is proportional to the work done by the compression. The work done by compression is approximately proportional to the product of load and axial strain in
Figure 19. Before the maximum load points of the specimens, the gravel specimen experienced the most frictional heat
. Therefore, according to Equation (4),
, the temperature change of gravel is higher than that of sand and clay.
For the clay specimen, during the plastic deform, there was significant radial deformation at the top and bottom of the specimen, which occurred immediately contact of the platen of the compression machine. Moreover, the rest of specimen deformed similar to an extremely viscous fluid. The friction results from the differential displacement rates between neighboring clay particles. For the sand specimen, as the specimen bulges, the sand particle layers must rearrange. Particles are squeezed into neighboring layers in an axial direction and hence friction occurs. As the friction is distributed among the entire specimen, thus
in unit mass is the least among the 3 cases during plastic deformation. For the gravel specimen, the
is more than 2 times that of the other two cases, because the friction concentrates on the global failure surface where two parts of the specimen slide against each other. The same set of curves except for that of the sand case are also replotted in
Figure 20 with normalized
. This shows that the affected distance of the crack in the clay case is less than that of the gravel case. This might be related to the particle size of the soil. As can be seen in the case of gravel, the surface of the temperature rise propagates through the ice in the voids of the soil particle skeleton. Moreover, the estimated specific heat of gravel was less than half of that of frozen clay. This reveals that it took less amount of heat for the frozen gravel to increase a unit of temperature than for the frozen clay. Thus, the temperature increase due to frictional heat occurred in a smaller spatial dimension in frozen clay than in frozen gravel.