1. Introduction
The area of permafrost worldwide accounts for approximately 20% to 25% of land area. The global permafrost is mainly distributed in the northern hemisphere, especially in high-altitude areas such as Russia and Canada, as well as China, such as the Qinghai Tibet Plateau. The area of cold regions in China accounts for about 75% of the national territory. There are many cold regions in China, which are famous around the world [
1].
Frozen rock and frozen soil changes are global issues. As a major country with permafrost and frozen rock, the study of China’s frozen rock is not only a necessity for scientific exploration, but also a necessary measure to address the challenges of climate change and ensure infrastructure security. It is also a necessary path to maintain ecological balance and sustainable socio-economic development. The study of the characteristics of frozen rocks in China is of great significance.
As part of its ongoing initiatives under the “Belt and Road” and “Western Development” strategies, China has been instrumental in initiating a multitude of projects in the colder regions such as Xinjiang and Xizang. These efforts, consistent with national policies [
2,
3], have led to significant development activities in these areas [
4]. However, in some areas, the rock masses are constantly frozen. Due to the complexity of the geological environment, there are obvious differences in the internal water content of rocks during diagenesis. Variations in water content and levels of saturation significantly influence the physical and mechanical characteristics of rock masses in cold regions [
5,
6,
7,
8]. Furthermore, rock masses in these frigid areas are exposed to not only static loads but also dynamic influences such as blasting and mechanical construction activities [
9,
10]. Consequently, an in-depth analysis of the static mechanical properties of frozen rocks under different temperatures and saturation levels is vital for the effective management of rock mass stability in these cold environments. During tunnel excavation and blasting construction in these cold regions, it is possible to have a better understanding of rock characteristics and avoid unnecessary geological hazards.
Previous research endeavors have delved into the mechanical behaviors of rock specimens at low temperatures, with a focus on the mechanical attributes of frozen rock. These studies have primarily utilized methods such as indoor uniaxial compression, shear resistance evaluation, and Brazilian splitting tests to investigate these properties [
11,
12,
13]. In particular, the article of Wang Chao [
14] has centered on the analysis of residual deformation. This research involved subjecting a soil–rock mixture to multiple cycles of freezing and thawing. Findings from this research indicate that during freeze–thaw cycles, the soil–rock mixture undergoes repeated processes of frost heaving and thaw-induced contraction. It was observed that the initial instances of frost heave and thaw shrinkage exhibited significant changes. However, as the number of freeze–thaw cycles increased, a decrease in residual deformation was noted. Finally, the residual deformation tends to stabilize. Lv Zhitao [
15] conducted a frost heave test on saturated sandstone, which exhibited open cracks. Investigations have revealed that in environments where freezing occurs uniformly, the phenomenon of frost heave in the fissures of highly permeable sandstone is more significant when contrasted with scenarios of unidirectional freezing. The interplay between the freezing dynamics and the permeability characteristics of the rocks plays a pivotal role in influencing the alterations in the water content within these fissures. So, different permeable rocks will produce different crack and frost heave modes under different freezing conditions. Zhu Chuanqu [
16] studied the strength characteristics and mechanism of coal rock interface freezing through indoor experiments. A comprehensive set of direct shear experiments was performed on frozen coal and rock specimens under varying conditions of temperature, moisture content, and normal stress. Experimental findings indicate that the moisture level significantly affects the strength at the junction where coal and rock are frozen together. A notable increase in this strength was observed with rising moisture levels. For instance, during experiments conducted at a temperature of −10 °C, the frozen rock’s strength notably enhanced from 75.46 KPa to 267.42 KPa when moisture levels were elevated from 3% to 9%. Additionally, in a separate research study, Wang Ting [
17] explored the pressure-melting phenomenon in frozen sandstone. This was done by conducting uniaxial compression tests and concurrently observing alterations in the electrical resistance within the sandstone. The findings showed that during the microcrack compaction stage, the electrical resistance of saturated frozen rock drops rapidly with increasing strain. However, during the elastic deformation and microcrack propagation stages, the resistance of sandstone decreases more gradually, contrasting notably with dry rocks. Furthermore, Wang Tingting [
18] undertook laboratory-based Brazilian splitting tests to assess the tensile characteristics of fractured rock masses in cold environments that have undergone freezing. The research findings suggest that frozen rock specimens display characteristic brittle failure properties. There is a gradual decline in the tensile strength of frozen rock as the dimensions of cracks, both in width and length, increase.
Research has been conducted on the impact of water content on rock mechanical properties. Uniaxial compression, tensile, and direct shear tests were performed on specimens with varying moisture contents to analyze water’s weakening effect on rock strength [
19,
20,
21,
22]. Zhou Kunyou [
23] investigated the impact of water content on rock strength through a series of uniaxial compression and tensile tests. The results indicated that water content significantly reduces the mechanical strength of rocks, transitioning their failure mode from a mixed tensile–shear type to predominantly tensile. Li Bo [
24] performed direct shear tests on granite and sandstone specimens, which exhibited serrated fracture cracks. The rock specimens were subjected to three moisture conditions: dry, surface wet, and saturated. Findings suggest that surface moisture only alters the basic friction angle, while saturation leads to a reduction in both the unconfined compressive strength and basic friction angle of the rock specimens. Li Diyuan [
25] established two parameters, namely the change in critical saturation and saturation per unit length, to analyze the rate of decline in rock strength and describe the distribution of water in cylindrical specimens. Using these two parameters, an analytical model was developed for calculating the normalized unconfined compressive strength of rocks with varying saturation levels. This model was applied to a tunnel project located in a fault zone in Yunnan as a case study. Kang Yongshui [
26] focused on the mechanical properties of rock joints with a high content of clay. The findings from these experiments highlighted that the moisture content in the clay filler considerably affects the shear strength of the rock joint. Research has indicated that beyond the plastic limit of moisture content, there exists a negative correlation between the level of water content and the shear strength observed in rock joints.
Currently, many scholars have studied the mechanical properties of frozen rocks. Some scholars have also studied the influence of water content on the mechanical properties of rocks. However, the mechanical properties of rocks in a frozen state under different water content conditions are rarely studied by anyone. In cold regions, the mechanical properties of rocks are related to both low temperature and water content. So, it is necessary to explore the synergistic effect of low temperature and water content on rocks. Especially at low temperatures, the influence of different water contents on the mechanical properties of rocks is important. The influence of different low temperatures on the mechanical properties of rocks is also important under certain moisture content conditions. This study aims to evaluate the mechanical behavior of rock specimens subjected to different temperature and moisture conditions through uniaxial compression tests. This evaluation includes an examination of various aspects such as failure morphology, stress–strain responses, UCS, EM, and additional alterations in the rock specimens. This paper focuses on the influence of water content and low temperature on the mechanical properties of rocks. Special attention should be paid to the failure modes of rocks with different water contents at low temperatures.
4. Discussion
In this paper, we divided specimens into three groups for experiments and conducted a total of 42 experiments. All experimental results are listed in
Table A1 in
Appendix A. The scope of our experiments encompassed an investigation into the impact of low temperatures on the mechanical properties of rock specimens. Additionally, we examined how varying water contents affect these properties at an ordinary temperature of 8 °C, as well as at a low temperature of −5 °C. Each set of tests was analyzed to determine the macroscopic fracture characteristics and static strength characteristics of the rock specimens. Investigations into the influence of sub-zero temperatures and moisture levels on the structural integrity of rock specimens, particularly in terms of crack quantity and shape, remain notably scarce from other papers. This study’s findings hold considerable value for guiding construction projects in permafrost zones and hydrous rock formations, especially under conditions where fissures filled with water are prevalent in rocks in cold climates. The importance of acknowledging the decrease in the strength and ductility of rock masses under these circumstances cannot be overstated.
The study conducted by Zhao Yangchun [
27] highlights a notable increase in the peak strength of frozen sandstone with a decrease in temperature, aligning with the outcomes presented in this research. Observations indicate a positive correlation between lower temperatures and the enhancement of UCS and EM in rock specimens. This strengthening and increased brittleness of rock specimens can be attributed to the solidification of water within their pores, resulting in a gradual augmentation of the EM of the pore ice. Consequently, this process elevates the overall relative EM of the rock. Furthermore, the amplification of strength in these frozen rocks can also be linked to the contraction of minerals present within the rocks, as noted in reference [
28]. At the same time, Zhao Yangchun proposed, “With the temperature decreasing, the non-linear behavior of yield stage weakens”. This is consistent with our suggestion that as the temperature decreases, the rock specimen gradually transforms from a plastic–elastic–plastic body to a plastic–elastic body. This is due to the shrinkage and deformation of the rock skeleton caused by low temperatures, leading to the closure of some pores [
29]. The rock becomes denser. The process of the rock yielding stage is shortened.
Therefore, through analysis, we can know that the increase in uniaxial compressive strength and elastic modulus of rocks at low temperatures is mainly due to the solidification of water in the rocks at low temperatures. Due to the solidification of water, its volume expands and fills the pores in the rock, as shown in
Figure 16. At the same time, the skeleton and particles of the rock may shrink at low temperatures [
30]. The rock becomes denser at low temperatures, so its strength increases.
In our study, it was observed that both the uniaxial compressive strength (UCS) and the EM of the rock specimens exhibited a decline as the moisture content increased. This heightened level of moisture was found to adversely affect the strength of these rock specimens. At the ordinary temperature, the strength of rocks saturated with water was reduced by 40.8%, compared to dry rocks. This indicates that the presence of water can have a deteriorating effect on the mechanical properties and stability of rock masses. The gradual dissolution of the binding substances within the rock due to water exposure results in a diminished bonding force among the mineral particles of the rock [
31]. This process ultimately leads to a reduction in the rock’s strength [
32]. Tomor AK [
33] noted in his research that there was a significant decrease in the UCS of sandstones when subjected to varying moisture levels. Specifically, it was observed that Darney stone lost 50% of its UCS under conditions of air dryness. The findings of Tomor AK corroborate the conclusions drawn in this study. However, on the basis of his research, this article also adds an analysis of the influence of water content on the mechanical properties of rocks at low temperatures. The study observed that the weakening effect of water on rock strength is amplified under low-temperature conditions, which can be attributed to the simultaneous presence of water, ice, and rock within the specimen at these temperatures [
34]. Each component exhibits distinct temperature sensitivity, leading to uneven contraction of the rock specimens [
35]. This differential response significantly influences the initiation and expansion of new microcracks [
36].
So, an increase in the water content of rocks will lead to a weakening of their strength. At an ordinary temperature, the water inside the rock will dissolve a portion of the cementing substance to weaken its bonding strength. At low temperatures, various substances inside rocks will contract or expand in different ways. Uneven shrinkage of rocks can lead to the expansion of existing cracks or the generation of new cracks. As shown in
Figure 17, with the increase in water content inside the rock, the cement inside the rock is dissolved and the number of cracks inside the rock also increases.
This study assessed the mechanical behavior of rocks under varying low-temperature and moisture conditions. It was observed that lower temperatures generally enhance the mechanical robustness of rocks while simultaneously increasing their brittleness. Furthermore, the presence of water was found to reduce rock strength, an effect that was more pronounced in low-temperature environments. The insights and conclusions derived from this research offer valuable guidance for future studies on the dynamic mechanical properties of rocks in cold and moist conditions.