Detection and Spatio-Temporal Distribution of Pinnatoxins in Shellfish from the Atlantic and Cantabrian Coasts of Spain
Abstract
:1. Introduction
2. Results
3. Discussion
4. Material and Methods
4.1. Chemicals and Solvents
4.2. Sampling
4.3. Extraction and Sample Preparation
4.4. LC-MS/MS Analysis
4.5. Statistical Analysis
Supplementary Materials
Author Contributions
Funding
Acknowledgments
Conflicts of Interest
References
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Toxin | Ionisation | Parent Ion | MS/MS Transition | CE (eV) | Cone Voltage (V) | |
---|---|---|---|---|---|---|
PnTX A | ESI+ | [M + H]+ | 712.5> | 164 | 50 | 60 |
712.5> | 440.3 | 36 | 60 | |||
712.5> | 538.3 | 36 | 60 | |||
712.5> | 694.5 | 36 | 60 | |||
PnTX BC | ESI+ | [M + H]+ | 741.5> | 164 | 50 | 60 |
741.5> | 458.3 | 36 | 60 | |||
741.5> | 723.5 | 36 | 60 | |||
PnTX D | ESI+ | [M + H]+ | 782.5> | 164 | 50 | 60 |
782.5> | 446.3 | 36 | 60 | |||
782.5> | 764.5 | 36 | 60 | |||
PnTX E | ESI+ | [M + H]+ | 784.5> | 164 | 57 | 60 |
784.5> | 446.3 | 41 | 60 | |||
784.5> | 766.5 | 57 | 60 | |||
PnTX F | ESI+ | [M + H]+ | 766.5> | 164 | 50 | 60 |
766.5> | 446.3 | 36 | 60 | |||
766.5> | 748.5 | 36 | 60 | |||
PnTX G | ESI+ | [M + H]+ | 694.5> | 164 | 50 | 60 |
694.5> | 440.3 | 36 | 60 | |||
694.5> | 676.5 | 36 | 60 | |||
PnTX H | ESI+ | [M + H]+ | 708.5> | 164.2 | 57 | 60 |
708.5> | 690.4 | 57 | 60 |
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Lamas, J.P.; Arévalo, F.; Moroño, Á.; Correa, J.; Muñíz, S.; Blanco, J. Detection and Spatio-Temporal Distribution of Pinnatoxins in Shellfish from the Atlantic and Cantabrian Coasts of Spain. Toxins 2019, 11, 340. https://doi.org/10.3390/toxins11060340
Lamas JP, Arévalo F, Moroño Á, Correa J, Muñíz S, Blanco J. Detection and Spatio-Temporal Distribution of Pinnatoxins in Shellfish from the Atlantic and Cantabrian Coasts of Spain. Toxins. 2019; 11(6):340. https://doi.org/10.3390/toxins11060340
Chicago/Turabian StyleLamas, J. Pablo, Fabiola Arévalo, Ángeles Moroño, Jorge Correa, Susana Muñíz, and Juan Blanco. 2019. "Detection and Spatio-Temporal Distribution of Pinnatoxins in Shellfish from the Atlantic and Cantabrian Coasts of Spain" Toxins 11, no. 6: 340. https://doi.org/10.3390/toxins11060340
APA StyleLamas, J. P., Arévalo, F., Moroño, Á., Correa, J., Muñíz, S., & Blanco, J. (2019). Detection and Spatio-Temporal Distribution of Pinnatoxins in Shellfish from the Atlantic and Cantabrian Coasts of Spain. Toxins, 11(6), 340. https://doi.org/10.3390/toxins11060340