1. Introduction
Shale, as a common sedimentary rock, has a layered structure formed by an ordered parallel arrangement of a high-strength rock matrix and low-strength bedding planes [
1,
2]. Due to the different physical and mechanical properties of the rock matrix and bedding planes, there are significant differences in the mechanical and deformation properties of the shale between the parallel bedding planes direction and the vertical bedding planes direction, resulting in the macroscopic mechanical properties of shale being controlled by bedding planes, exhibiting significant anisotropic mechanical characteristics [
3,
4,
5]. Excavating a tunnel in shale formations can cause disturbances to the surrounding rock mass, leading to the opening or sliding of the bedding planes within the shale, reducing its macroscopic mechanical parameters such as strength and modulus, resulting in damage and deterioration of surrounding rock mass [
6]. This leads to engineering disasters such as tunnel collapse, asymmetric large deformation, and support cracking, which not only seriously affects the construction progress, but also endangers construction safety. Therefore, it is vital to systematically investigate the anisotropic mechanical properties of shale under triaxial loading, which is meant to provide a theoretical basis for the design of support and excavation parameters for tunnels in shale or other layered rock formations.
Anisotropy of rock materials refers to the characteristics of mechanical parameters, structural properties, and constitutive relationships that change with direction, and numerous scholars have carried out studies on the anisotropy of rock materials [
7,
8,
9]. Meanwhile, shale is often known for its remarkable intrinsic anisotropic properties, including strength, brittleness, acoustic velocity, permeability, fracture toughness, etc. [
10,
11,
12,
13,
14,
15]. Various studies have first focused on the anisotropy of the basic mechanical properties of shale. For example, Lo et al. [
16] studied the elastically anisotropy of Chicopee shale and found that the elastic anisotropy of shale is due to the combined effects of pores or cracks and mineral grain orientation and decreases with increasing confining pressure. Niandou et al. [
17] investigated the anisotropic mechanical behavior of the Tournemire shale and found that the plastic deformation and failure mode of the Tournemire shale is anisotropic and strongly depends on confining pressure. Geng et al. [
18] addressed that the brittleness anisotropy of Longmaxi shale samples was bedding angle-dependent, and the anisotropy of brittleness decreased with increasing confining pressure through the triaxial experiments under various confining pressure. Yang et al. [
19] conducted an experimental study on the mechanical behavior and brittleness characteristics of Longmaxi shale, and the anisotropic behavior of shale specimens under conventional triaxial compression, including the strength, brittleness, deformation, and failure behaviors, was analyzed. Wang et al. [
20] studied the damage evolution and acoustic emission (AE) characteristics during failure process of anisotropic shale and revealed the effect of different layer inclination angles between the loading direction and the bedding planes. Ma et al. [
21] analyzed the characteristics of the anisotropic tensile strength of layered rocks and three different anisotropic tensile failure criteria were reviewed and compared. Zhang et al. [
22] investigated the tensile mechanical properties and damage patterns of shale with different various orientations of the bedding planes by conducting a Brazilian splitting test and an AE test. Wang et al. [
23] conducted a high-temperature triaxial permeability testing machine to study anisotropic permeability of oil shale at stresses that emulate in situ conditions. Mayr et al. [
24] proposed the porosity deformation approach (PDA) to the elastic anisotropy of shale under triaxial loading and found that the velocity change due to hydrostatic loading can be used to predict elastic anisotropy under additional axial loading. Wilczynski et al. [
25] studied the anisotropy of strength and elastic properties of lower Paleozoic shales from the Baltic basin, Poland, and found that the shale was characterized by VTI type (vertical transverse isotropy) internal anisotropy. Xu et al. [
26] adopted a finite-element–based continuum damage mechanics model to capture sample size effects and the influence of intrinsic anisotropy on the stress–strain response of shale and investigated deformation and stiffness anisotropy induced by damage propagation in a rock brittle deformation regime. Xie et al. [
27] studied the anisotropic characteristics of the failure mechanism by conducting AE monitoring tests on shale specimens with seven different bedding inclination angles under uniaxial cyclic loading and unloading. Kong et al. [
28] explored the anisotropy of the mechanical properties of shale and the energy evolution of its failure through the cyclic loading and unloading experiments of shale specimens with seven different bedding orientations.
On the other hand, in terms of dynamic mechanical properties of shale, some efforts had also been conducted to investigate the mechanical properties of shale under dynamic loads with different strain rates, including anisotropic characteristics of strength, elastic modulus, failure mode, etc. [
29,
30,
31,
32,
33,
34]. In addition, geologists engaged in the development of unconventional shale gas and shale oil had carried out a lot of research on the anisotropy of elastic wave velocity of shale. Vernik et al. [
35] implemented ultrasonic velocity and anisotropy measurements on a variety of shale with different clay and kerogen content, clay mineralogy, and porosity at a wide range of effective pressure, and found that the elastic anisotropy of shale increased substantially with compaction. Kuila et al. [
36] investigated the ultrasonic velocity response of low porosity shale in Western Australia to both isotropic and anisotropic stress fields and to evaluate the velocity response to the changing stress field. Wang et al. [
37] conducted real-time ultrasonic and mechanical experiments of Longmaxi formation shale under uniaxial deformation; the results suggest that shale govern the intrinsic P- and S-wave velocity anisotropy, and pronounced bedding planes have a significant influence on the mechanical properties and velocity responses of shale. Dewhurst et al. [
38] performed multiple stage triaxial tests of Norwegian Sea shale and evaluated rock strength and the evolution of ultrasonic response during rock deformation. They found that the S-wave anisotropy was significantly affected by the increasing stress anisotropy. Zhubayev et al. [
39] studied the velocity and attenuation anisotropy of P- and S-waves in dry Whitby Mudstone samples as a function of stress by ultrasonic experiments and found the degree of anisotropy to be as large as 70% for velocity and attenuation, and the sensitivity of P-wave anisotropy change with applied stress to be more conspicuous than for S-waves.
Meanwhile, hydraulic fracturing is the key technology for efficient exploitation of shale gas and oil [
40,
41,
42]. In the process of hydraulic fracturing, the initiation and propagation of hydraulic fractures is controlled by the fracture toughness of shale. As an anisotropic material, the fracture toughness of shale varies in different directions. Chandler et al. [
43] conducted fracture toughness measurements on Mancos shale determined in all three principal fracture orientations using a modified short-rod methodology, and significant anisotropy was observed in shale fracture toughness measurements. Kramarov et al. [
44] measured the anisotropic nature of mode I fracture toughness of Mancos shale by combining semi-circular bend test (SCB) and digital image correlation (DIC), and the experiments were carried out in different notch orientations with respect to bedding. Inskip et al. [
45] characterized fracture toughness from Nash Point shale in multiple orientations, including angles oblique to the three principal fracture orientations, and found that the fracture toughness of Nash Point shale is mechanically highly anisotropic. Shi et al. [
46] employed shale samples with different bedding angles (the angle between loading axis and bedding planes) for cracked chevron notched Brazilian disc test (CCNBD) and Brazilian disc test, to characterize the bedding-plane-induced fracture toughness anisotropy in shale and its relationship with other physical and mechanical properties. Guo et al. [
47] carried out a series of fracture experiments on the Longmaxi shale specimens with five bedding orientations after constructing in situ temperatures, and the results revealed that increasing in situ temperature decreases the fracture toughness but increases the fracture toughness anisotropy. Wang et al. [
48] utilized real-time ultrasonic detection and post-test CT imaging to reveal anisotropic energy and ultrasonic characteristics of black shale under triaxial deformation, indicating that the strain energy evolution and fracture anisotropy were bedding orientation dependent.
In summary, although some scholars have studied the intrinsic anisotropic properties of shale, there is still no clear and unified understanding of the shale’s anisotropic mechanical behaviors under triaxial loading. Thus, it is necessary to systematically investigate the anisotropic mechanical properties of shale under triaxial loading, which is meant to provide reference basis for the design of tunnel excavation and support in shale formation. In this work, the composition and microstructure of shale in western Hubei were tested using XRD and SEM, and then a uniaxial AE compression test and triaxial compression test were carried out. Moreover, the anisotropy characteristics of shale’s compressive strength, deformation parameter, and failure modes were studied, as well as the anisotropic index of shale’s mechanical parameters. Finally, the reason for the mechanical anisotropy of shale under triaxial loading was discussed in detail.
4. Analysis of Anisotropic Mechanical Characteristics of Shale
According to the results of the uniaxial and triaxial tests of the shale, it can be found that mechanical parameters such as the strength and modulus of shale samples with different bedding angles show significant anisotropy. Therefore, this section focuses on analyzing the anisotropy of mechanical behavior of shale samples and the reasons for its occurrence.
4.1. Compressive Strength Anisotropy of Shale
The compressive strength of all the shale samples with different bedding structures obtained from uniaxial and triaxial compression tests are sorted out, and the average values of the compressive strength of shale samples under the same loading condition are used as the compressive strength
σcs to carry out anisotropic analysis; meanwhile, the relationship curves of compressive strength
σcs and bedding angle
θ with confining pressure
σ3 are drawn, as shown in
Table 2 and
Figure 6.
As shown in
Table 2 and
Figure 6a, the compressive strength
σcs of the shale samples exhibits significant anisotropy, and
σcs under the same confining pressure
σ3 shows a “U-shaped” trend of first decreasing and then increasing with the increase in the bedding angle
θ. Secondly, the minimum value of
σcs of shale samples with or without confining pressure
σ3 is achieved at the bedding angle of 60°, which is consistent with the experimental results of other researchers [
9,
17,
19]. On the other hand, with the increase in confining pressure, the bedding angle
θ corresponding to the maximum value of
σcs tends to change from 0° to 90°. When confining pressure
σ3 is between 0 MPa and 30 MPa, the bedding angle corresponding to the maximum value of
σcs is obtained at 0°, while at the higher confining pressure of 40 MPa, the maximum value is obtained at a bedding angle of 90°. It can be seen that the sensitivity of
σcs to the confining pressure under different bedding angles is different.
In addition, the compressive strength
σcs of shale samples at the same bedding angle
θ mostly increases with the confining pressure
σ3, which conforms to the effect of confining pressure in the traditional rock triaxial test, as shown in
Figure 6b. Moreover, within the confining pressure
σ3 range of 0 MPa to 40 MPa in the test, the compressive strength
σcs and confining pressure
σ3 show an approximate linear relationship. Therefore, the curve between compressive strength
σcs and confining pressure
σ3 in
Figure 6b is fitted by Equation (1), and the coefficient
A and
B in Equation (1) represent the sensitivity of compressive strength of confining pressure at this bedding angle and the uniaxial compressive strength, respectively.
Table 3 shows the values of coefficient
A and
B obtained by linear fitting of the experimental data according to Equation (1). It is worth noting that some abnormal data in
Figure 6b were excluded in the fitting process. The reason why these data are considered abnormal is that they violate the trend of rock compressive strength increasing with the confining pressure in traditional rock triaxial tests, which is also followed by most of the data in the triaxial tests in this paper. Therefore, in order to ensure that the fitted equation can be applied to most test data, and to increase the accuracy of linear fitting (that is, to improve the value of R-square) and the safety of subsequent strength criteria, some abnormal data are removed, as shown in
Table 3, and the fitting index R-square before and after abnormal data are removed is also given in the table.
As can be seen from
Table 3,
R-square values are all greater than 0.95, indicating that the linear relationship between shale compressive strength
σcs and confining pressure
σ3 is very significant after removing some abnormal data. The fitting curve and the measured data are drawn in
Figure 7, and it is not difficult to find that due to the difference in the sensitivity coefficient of bedding angle
θ, the critical point of confining pressure is about 35 MPa between the shale compressive strength at a 90° bedding angle and the shale compressive strength at a 0° bedding angle. When the confining pressure
σ3 is near the critical point, the bedding angle corresponding to the maximum shale strength will be transformed.
According to the linear relationship between compressive strength
σcs and confining pressure
σ3 of shale, it can be considered that the shale samples with different bedding angles basically obey the Mohr–Coulomb strength theory under the minimum principal stress of nearly 0~40 MPa, and the principal stress expression of Mohr–Coulomb strength theory is as shown in Equation (2).
where
c is cohesion and
φ is the internal friction angle. According to the data in
Table 2, the values of
c and
φ of shale samples with five bedding angles are shown in
Table 4.
Figure 8 shows the variation of the cohesion
c and the internal friction angle
φ of the shale samples with the bedding angle
θ. It can be seen that the
c and
φ of samples decrease first and then increase with the increase in the bedding angle
θ, and both obtain the minimum value when the bedding angle
θ is 60°, which is the same as the variation of compressive strength
σcs with the increase in bedding angle
θ. The difference is that the maximum cohesion
c obtained when
θ is 0°, while the maximum internal friction angle
φ is obtained when
θ is 90°.
4.2. Compressive Deformation Parameter Anisotropy of Shale
Modulus and Poisson’s ratio are the main parameters used to characterize the compressive deformation characteristics of rock, and the elastic modulus
Eθ, 50% strength deformation modulus
E50, and Poisson’s ratio
vθ of shale with different bedding angles are discussed, respectively. The average values of shale compressive deformation parameters measured by uniaxial and triaxial compression tests are shown in
Table 5.
According to
Table 5, the values of elastic modulus
Eθ and 50% strength deformation modulus
E50 are close when the confining pressure
σ3 is no less than 20 MPa, but there are some differences when the confining pressure is lower than 20 MPa. The reason for this phenomenon is that the compaction stage of shale stress–strain curve under low confining pressure conditions has different effects on the calculation process of these two moduli. The
Eθ is calculated based on the straight section of the stress–strain curve, which reflects the deformation of rock in the linear elastic stage. However, the
E50 reflects the average deformation of rock in the early compaction stage, and its value will be affected by the compaction stage, so is slightly lower than
Eθ. The ratio of elastic modulus
Eθ to the 50% strength deformation modulus
E50 of shale samples under different confining pressures are listed in
Table 6, and it can be found that with the increase in the confining pressure applied synchronously in the first stage of the triaxial compression test, the value of
Eθ/
E50 rises and approaches 1, indicating that the compaction stage of the shale samples is gradually shortened. At the same time, when the confining pressure
σ3 is greater than 20 MPa, the values of
Eθ/
E50 of shale samples at five bedding angles are all close to 1, showing that shale samples can be fully compacted under the action of confining pressure
σ3.
On the other hand, according to
Table 5, it can be found that with the increase in confining pressure, the elastic modulus
Eθ and 50% strength deformation modulus
E50 both increase, and the changes are similar. Therefore, only the variation of elastic modulus
Eθ with confining pressure
σ3 is analyzed, and the change curve of elastic modulus
Eθ with respect to confining pressure
σ3 is sorted out, as shown in
Figure 9.
It can be found from
Figure 9 that the elastic modulus
Eθ with confining pressure
σ3 show an approximate linear growth relationship, so the
Eθ and
σ3 are linearly fitted, and the obtained linear fitting parameters and fitting index
R-square are listed in
Table 7, and the linear fitting equation is shown in Equation (3).
where
C and
D represent the sensitivity of shale elastic modulus
Eθ to confining pressure
σ3 and the uniaxial compressive elastic modulus of shale at this bedding angle.
It can be seen from
Table 7 that the fitting index
R-square of linear fitting between the elastic modulus
Eθ and confining pressure
σ3 of shale samples with different bedding angles are close to or greater than 0.8, indicating that
Eθ and confining pressure
σ3 basically obey a linear relationship. The comparison between the linear fitting function and the experimental results is sorted out, as shown in
Figure 10. It can be observed that the sensitivity of the
Eθ to the confining pressure effect is different under various bedding angles. Combined with the sensitivity coefficients in
Table 3 and
Table 7, it is found that the variation of shale elastic modulus
Eθ sensitivity to confining pressure
σ3 with bedding angle
θ is very similar to that of the compressive strength
σcs sensitivity. The sensitivity coefficient
C decreases slowly in the bedding angle
θ range of 0°~60°, and the growth of elastic modulus
Eθ decreases gradually with the increase in confining pressure
σ3, while the sensitivity coefficient increases rapidly in the range of 60°~90°, showing that the growth of
Eθ increases rapidly with the confining pressure
σ3.
In addition to the elastic modulus
Eθ, Poisson’s ratio is also a very important elastic constant, and the variation curves of Poisson’s ratio
vθ and confining pressure
σ3 of shale samples obtained by uniaxial and triaxial tests are shown in
Figure 11, and it can be found that the variation of Poisson’s ratio
vθ of shale with confining pressure
σ3 is disordered. According to the transverse isotropic properties and the experimental scheme, the Poisson’s ratio
vθ of shale samples with a bedding angle of 0° measured by the chain extensometer is a constant, while the
vθ measured by the samples with other bedding angles are all mixed data of
vθ in different directions. Therefore, only the relationship between
vθ and confining pressure
σ3 for samples with a bedding angle of 0° is discussed. As shown in
Figure 11,
vθ and
σ3 for shale samples with a bedding angle of 0° are approximately positively correlated.
On the other hand, according to the data in
Table 5, the variation curves of elastic modulus
Eθ and 50% strength deformation modulus
E50 of shale samples with bedding angle
θ under different confining pressures
σ3 are drawn, as shown in
Figure 12.
It can be seen from
Figure 12 that the
Eθ and
E50 of shale have similar variation trends with the bedding angle, and the anisotropic characteristics are obvious. Both the
Eθ and
E50 show a changing trend of first decreasing and then increasing with the increase in the bedding angle
θ, and the variation is gentle when the bedding angle
θ is less than 45°, while the change is drastic when the angle is greater than 45°. Within the designed confining pressure range in the test, the maximum values of
Eθ and
E50 of shale are obtained when the bedding angle is 90°, while the bedding angle corresponding to the minimum value is basically 30°. In addition, the relationship between the Poisson’s ratio
vθ of shale and the bedding angle
θ in this experiment is unclear, so no further specific analysis is made.
4.3. Anisotropic Index of Shale’s Mechanical Parameters
Anisotropic index
Rc is an important parameter to quantitatively evaluate the anisotropic degree of the mechanical properties of materials. Singh et al. [
49] proposed a formula for calculating the anisotropic index
Rc of rock materials, which is the uniaxial compressive strength of the materials at a 90° bedding angle divided by the minimum uniaxial compressive strength of the rock materials within 0°~90° bedding angles, and the classification standard of anisotropic degree is also given, as shown in
Table 8.
The calculation method of the anisotropic index
Rc used in this paper adopts the calculation formula proposed by Niandou et al. [
17], as shown in Equation (4), and the anisotropic
Rc is calculated by the ratio of the maximum value to the minimum value of the physical and mechanical parameters of shale at different bedding angles. In this paper, the compressive strength
σcs and elastic modulus
Eθ of shale samples are selected for calculating anisotropic indexes, and
Table 9 shows the anisotropic indexes calculated by the
σcs and
Eθ of shale samples in
Table 2 and
Table 5.
According to the anisotropic indexes of the compressive strength
σcs of the shale, combined with the anisotropic grading standard in
Table 8, it is determined that the shale has a moderate degree of anisotropy. In the confining pressure
σ3 range of 0~40 MPa, the bedding angle
θ corresponds to the extreme values of the compressive strength
σcs and elastic modulus
Eθ of shale changes, which increases the complexity of analyzing the anisotropy. The fitting curves of the anisotropic indexes of
σcs and
Eθ with
σ3 are sorted out, as shown in
Figure 13, and the functional expressions of the fitting curves are shown in Equations (5) and (6).
For compressive strength
σcs, the fitting formula is as follows:
For elastic modulus
Eθ, the fitting formula is as follows:
According to
Figure 13, the anisotropic indexes of shale are obviously affected by confining pressure
σ3, and the anisotropic indexes of elastic modulus
Eθ are positively correlated with
σ3, while the anisotropic indexes of compressive strength
σcs are negatively correlated with
σ3 in the range of 0 to 35.314 MPa, and when the
σ3 is greater than 35.314 MPa, the indexes of compressive strength
σcs are positively correlated with
σ3. The reason is that the compressive strength of shale samples with a 90° bedding angle will increase rapidly with
σ3, and its growth rate is greater than that of the samples with a 0° bedding angle. When the
σ3 increases from 30 MPa to 40 MPa, the compressive strength of shale samples with a 90° bedding angle exceeds that of samples with a 0° bedding angle, which becomes the maximum compressive strength of shale with different bedding angles. As a result, the anisotropic index of compressive strength has a transition value between the
σ3 of 30 MPa and 40 MPa, that is, the minimum value. The anisotropy of strength and deformation parameters of shale samples is closely related to the obvious differences in layered structure and mechanical properties of constituent materials, and the macro failure mode of shale samples is also deeply related to the anisotropic characteristics.
4.4. Anisotropy Characteristics of Shale Compression Failure Modes
The strength and deformation characteristics of rock are closely related to the failure mode. Unlike isotropic materials, the failure modes of shale samples in uniaxial and triaxial compression tests are affected by the confining pressure
σ3 and the bedding angle
θ, and there are many kinds of failure modes.
Table 10 lists the failure modes of representative shale samples in uniaxial and triaxial compression tests, and the main fractures of the failure samples are marked by a red curve, and the bedding angle
θ of each sample is marked by a white straight line.
The composition of shale can be simplified into the shale matrix and bedding planes, and the failure modes of shale can be decomposed into four basic failure modes—tensile failure and shear failure of shale matrix and tensile failure and shear failure of bedding planes [
33]—while the different failure modes of shale samples presented in
Table 10 are combinations of these four basic failure modes. According to
Table 10, the following conclusions can be drawn:
(1) Consistent with isotropic materials, confining pressure σ3 can significantly change the failure modes of shale samples. Compared with triaxial compression, there are more penetrating fractures in shale samples under uniaxial compression, and their distribution is more complex. The reason for this phenomenon is that the uniaxial compression experiment lacks the constraint effect of radial stress.
(2) The uniaxial failure mode of the samples with a 0° bedding angle is a composite failure of tension and shear, and the friction cone at the end is the product of the hoop effect, and this failure mode is relatively complex, including four types of basic failure modes. With the application of confining pressure σ3, the failure mode of the samples with a 0° bedding angle changes to the through-bedding plane shear failure mode with a single fracture, and the fracture is not parallel to the bedding planes, which is the shear failure mode of rock matrix. In addition to the secondary fractures produced by uniaxial compression, the failure mode of samples with a 30° bedding angle is the same as that of samples with a 0° bedding angle, which is dominated by the shear failure mode of the shale matrix.
(3) The failure mode of the samples with a 45° bedding angle is mainly a composite failure mode of shear failure through the bedding planes and shear failure along the bedding planes. The failure surface of the composite failure mode is approximately composed of two failure angles; one is the angle of the bedding planes, and the other is the angle higher than the bedding angles. At the same time, a small number of shale samples with a 45° bedding angle also show pure shear failure mode along the bedding planes. The failure mode of the samples with a 60° bedding angle is mainly shear failure along the bedding planes. In addition, a small amount of composite shear failure between rock matrix and bedding planes occurs in samples with a 60° bedding angle.
(4) The failure mode of the shale samples with a 90° bedding angle is different from that of the samples with the other bedding angles; there are tensile cracks parallel to the bedding planes caused by the Poisson effect in the samples. Therefore, it can be considered that the failure mode of the samples with a 90° bedding angle belongs to the tensile failure mode of the bedding planes. As the confining pressure σ3 increases, some shear cracks through the bedding planes will appear on the samples. It can be seen that as the restraining of confining pressure σ3 on the tensile failure of bedding planes increases, the failure mode of the samples with a 90° bedding angle begins to gradually change into the shear failure mode of rock matrix.
5. Discussion
Based on the experimental results and analysis, the reason for the compressive strength σcs, elastic modulus Eθ, anisotropic index of σcs and Eθ, and failure modes of shale samples having different sensitivities to the variation of confining pressure σ3 is systematically analyzed:
(1) The reason for the σcs and Eθ of shale samples having confining pressure effects is that the spherical stress σm whose value is equal to σ3 has a compaction effect on the samples. Under the action of spherical stress σm, the microcracks inside the samples are closed, and the density, compressive strength σcs, and elastic modulus Eθ increase, which is the same for homogeneous rock and shale.
(2) The first difference is that the basic failure mode of shale changes from shear failure to tensile failure as the bedding angle
θ increases. According to
Table 10, it can be seen that the failure surface tendency of all samples is the same as the bedding planes’ tendency except for the samples with a 0° bedding angle, because shale is more prone to deformation along the bedding planes under deviatoric stress. Therefore, the three-dimensional stress condition of the samples can be simplified to the plane stress condition (ignoring the influence of the bedding planes’ direction), and it is easy to ascertain that the plane spherical stress
σm has a limited constraint effect on the shear stress generated by the deviatoric stress on the shear failure surface. The radial stress component of the spherical stress
σm can effectively suppress the radial strain of the samples, thereby reducing the possibility of the tensile failure of the sample. It is found that the spherical stress
σm has different restraining performance on the shear stress and radial strain, which are the main factors causing shear failure and tensile failure, and as the confining pressure increases from 0 to 40 MPa, the increase percentages of the compressive strength
σcs and elastic modulus
Eθ of the shale samples with bedding angles are 0°, 30°, 45°, 60°, and 90° are 62.8%, 88.87%, 86.7%, 114.1%, and 155.2% and 24%, 22%, 20.6%, 13.9%, and 33.9%, respectively, so the sensitivity of the shale samples with a high bedding angle (90°) dominated by tensile failure to the change in confining pressure is significantly greater than that of the samples with medium and low bedding angles (0°~60°) dominated by shear failure.
(3) The second difference is that the failure site of shale samples changes from the combination of the rock matrix and bedding planes to bedding planes. Combined with the failure images of shale samples shown in
Table 10 and the values of cohesion
c and internal friction angle
φ in
Table 4, it can be seen that the shear strength of the bedding planes is significantly weaker than that of the rock matrix. With the increase in the bedding angle, the shear failure characteristics of the samples are gradually dominated by the bedding planes, which leads to the phenomenon that the sensitivity of the shale samples to the change in confining pressure decreases when the basic failure mode is the shear failure. At the same time, it is observed that the failure modes of shale samples with 0°~30° low bedding angles are the same, so the sensitivity of compressive strength
σcs and elastic modulus
Eθ to confining pressure changes little in this range.
(4) The anisotropy index of the shale mechanical parameters is obviously affected by confining pressure, and the variation of anisotropy index of different mechanical parameters is different with the increase in confining pressure. Within the confining pressure range of the test, the anisotropic index of compressive strength basically decreases with the increase in confining pressure, while the anisotropy index of elastic modulus increases gradually. At present, it is generally believed that under a sufficiently high stress environment, the anisotropy of the rocks will gradually disappear and eventually tend to be isotropic, resulting in the anisotropy index of its mechanical parameters being close to 1. Therefore, combined with the experimental results in this paper, it can be concluded that with the increasing confining pressure, the anisotropy index of the mechanical parameters of shale does not monotonically decrease to 1.
(5) With the increase in confining pressure, the evolution of the failure modes of shale samples with different bedding angles under uniaxial and triaxial compression is as follows: 1. For the 0° bedding angle sample: The failure mode changes from a composite mode that includes both splitting failure perpendicular to the bedding planes and shear failure through the rock matrix to a shear failure mode through the rock matrix; 2. For the 30° bedding angle sample: The failure mode changes from a composite mode that includes both local splitting failure and shear failure through the rock matrix to a shear failure mode through the rock matrix; 3. For the 45° bedding angle sample: The failure modes of the samples are both a mixed mode that includes shear failure through the shale matrix and along the bedding planes; 4. For the 60° bedding angle sample: The failure mode changes from a composite mode that includes shear failure through the shale matrix and along the bedding plane to a shear failure mode along the bedding planes; 5. For the 90° bedding angle sample: The failure mode of the sample gradually evolved from the splitting failure along the bedding plane to the shear failure mode through the rock matrix. Therefore, it can be found that under different confining pressure conditions, although the failure modes of shale samples with different bedding angles have different evolution rules, the failure modes of shale samples all tend to evolve in the direction of shear failure mode through the rock matrix with the increase in confining pressure, and the anisotropy of the failure modes of shale samples with different bedding angles is gradually weakened.
6. Conclusions
(1) The AE characteristics of shale samples with different bedding angles in the compaction, elastic, plastic, and failure stages are significantly different during uniaxial loading, and the variation of AE hits, AE cumulative hits, and AE ringing counts with time are closely related to the angle between loading direction and bedding planes and the progressive failure mode of those samples.
(2) The uniaxial and triaxial compressive strength σcs of shale samples is anisotropic. Under different confining pressures, the compressive strength of shale samples first decreases and then increases with the increase in the bedding angle. The compressive strength of shale samples reaches the minimum value when the bedding angle is 60°, while the maximum values of compressive strength are obtained at the bedding angle of 0° when the confining pressure is 0~30 MPa and obtained at the bedding angle of 90° when the confining pressure is 40 MPa. At the same time, the compressive strength and confining pressure of shale samples with the same bedding angle conform to the linear growth relationship.
(3) The elastic modulus Eθ of shale samples also has anisotropic characteristics. Under the designed confining pressure, the elastic modulus of shale samples decreases first and then increases with the increase in the bedding angle, and the maximum values of elastic modulus are obtained when the bedding angle is 90°, while the bedding angle where the minimum value is located tends to increase gradually from 30° with the increase in confining pressure. The elastic modulus of shale samples with the same bedding angle has a linear growth relationship with confining pressure, while the variation of Poisson’s ratio with the bedding angle or confining pressure is disordered.
(4) According to the anisotropic grade of compressive strength σcs, the shale samples have moderate anisotropy. The variation of anisotropic index of compressive strength and elastic modulus of shale with confining pressure is different. In the confining pressure range of 0~35 MPa, the anisotropic index of compressive strength decreases with the increase in confining pressure, while the anisotropy index of elastic modulus increases gradually.
(5) The failure mode of shale samples is also anisotropic. In the uniaxial and triaxial experiment, the shale samples with 0° and 30° bedding angles mainly undergo through-bedding plane shear failure, and the samples with a 45° bedding angle mainly experience the composite failure of through-bedding plane shear failure and along-bedding plane shear failure. The failure mode of shale samples with a 60° bedding angle is mainly along-bedding plane shear failure, while the samples with a 90° bedding angle are dominated by tensile failure and will be accompanied by some tensile and shear cracks through the bedding planes under high confining pressures.