Sensitivity Analysis of Intensity-Modulated Plastic Optical Fiber Sensors for Effective Aging Detection in Rapeseed Transformer Oil
Abstract
:1. Introduction
2. Principles of Intensity-Modulated Fiber Optic Instrumentation
3. Materials and Methods
3.1. Sample Aging and Standard
- An oven capable of maintaining a constant temperature of 115 °C (ASTM D1934-20);
- Beakers;
- 18 × 1000 mL Pyrex narrow-mouthed conical flask;
- Natural ester TO (rapeseed);
- Aging timer;
- Distilled water;
- Copper (9 g) and paper (65 g) catalysts.
- Sample containers were meticulously prepared and designated with labels from S1 through S18. Conforming to the guidelines stipulated in ASTM D1934-20 [31], a sampling duration extending a minimum of 96 h was strictly maintained.
- A volume of 750 mL of pristine rapeseed oil was allocated to the container marked S1. In a similar manner, 750 mL of the identical oil specimen was allocated to each of seventeen (17) uncontaminated, narrow-mouthed conical flasks, culminating in a total of eighteen (18) samples with congruent mass. In adherence to ASTM D1934-20, and incorporating an amplification coefficient of 2.333′, this paralleled the recommended sampling ratio, encompassing a 300 mL test specimen situated within a 400 mL beaker, achieving an insulating depth of approximately 75 mm.
- The temperature of the oven was meticulously calibrated to register 115 ± 1 °C, followed by a pre-heating intermission spanning 120 s.
- Flasks, bearing labels from S2 through S18, were systematically introduced into the oven. Established sampling intervals were maintained. As a precautionary measure, protective hand gear was employed to mitigate thermal injuries. A structured aging schedule was punctiliously updated, reflecting the progressive removal of samples.
- Upon conclusion of the heating cycle, samples were permitted an adequate cooling period, reverting to ambient conditions.
- The contents housed within flasks S2 to S18 were systematically transferred to their respective designated containers (see Figure 1). It was imperative to ensure that these containers remained shielded from direct solar exposure.
- A thorough cleaning regimen was implemented for flasks S2 through S18, involving washing, rinsing, and subsequent drying.
3.2. Refractive Index Measurement
- Fresh and aged rapeseed ester oil;
- Bellingham + Stanley refractometer;
- Pipette;
- Clean, lint-free cloth;
- Distilled water;
- Fisher Scientific ethanol (99%+).
- The refractometer was adjusted to a RI value of 1.3333 utilizing distilled water for calibration purposes;
- Ethanol, applied with a lint-free cloth, was used to meticulously cleanse the prism of the refractometer;
- A fresh oil specimen was dispensed onto the prism using a pipette;
- By closing the refractometer’s lid, the oil was uniformly distributed across the prism’s surface (see Figure 2);
- The RI was ascertained by examining it through the device’s eyepiece;
- The process from steps 2 through 5 was reiterated for samples that had undergone aging;
- All recorded RI values were methodically logged, followed by a thorough cleaning of the refractometer and the testing area.
3.3. Fiber Optic Instrumentation Setup and Data Acquisition System
- Arduino Mega 2560 microcontroller;
- Light-emitting diodes (LED) (infrared, red, blue, and green);
- Optically insulated fabricated vessel for oil;
- 1000 µm uncladded plastic fiber optic cable;
- Phototransistor;
- Resistors;
- PC workstation + MATLAB software R2021a;
- Connecting cables;
- Fisher Scientific isopropyl alcohol (99.5+%).
- The opto-electronic setup was completed, as illustrated in Figure 3.
- The sensing area of the optical fiber sensor was cleaned with isopropyl alcohol to eliminate any contaminants or residual traces of TO.
- The optical fiber sensor underwent calibration, utilizing air as the reference fluid. The resulting transduced output voltage, as shown in Table 1, served as the calibration fluid for deviation adjustments during measurements of both fresh and aged samples. The setup was calibrated to the reference voltage in Table 1 before introducing each sample, ensuring that the results accurately reflected the sample characteristics.
- Then, 127 g of the fresh oil sample was poured into the optically insulated fabricated vessel.
- A settling time of one minute was observed before the transduced output voltage time series data were retrieved from MATLAB Simulink R2021a.
- Steps 2 to 5 were repeated for the aged samples.
- The voltage trend data for all samples were recorded and saved for subsequent analysis.
4. Results
4.1. Refractive Index Characterization
4.2. Sensitivity Analysis
4.2.1. Impact of Optical Source Wavelengths
4.2.2. Noise Response Analysis
4.2.3. Impact of Sensing Lengths
4.3. Repeatability of Results
5. Discussion, Conclusions and Future Studies
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
Abbreviations
ABP | Aging by-products |
ASTM | American Society for Testing and Materials |
DAQ | Data acquisition system |
LED | Light-emitting diode |
PMMA | Polymethyl methacrylic |
POF | Plastic optical fiber |
RI | Refractive index |
SOH | State of health |
TO | Transformer oil |
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Sensing Lengths (cm) | LEDs Calibration Voltage (V) | |||
---|---|---|---|---|
Green | Red | Blue | Infrared | |
1.5 | 4.99 | 4.99 | 4.99 | 4.9093 |
2.0 | 4.99 | 4.99 | 4.99 | 4.7488 |
3.0 | 4.99 | 4.99 | 4.99 | 4.1563 |
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Elele, U.; Nekahi, A.; Arshad, A.; McAulay, K.; Fofana, I. Sensitivity Analysis of Intensity-Modulated Plastic Optical Fiber Sensors for Effective Aging Detection in Rapeseed Transformer Oil. Sensors 2023, 23, 9796. https://doi.org/10.3390/s23249796
Elele U, Nekahi A, Arshad A, McAulay K, Fofana I. Sensitivity Analysis of Intensity-Modulated Plastic Optical Fiber Sensors for Effective Aging Detection in Rapeseed Transformer Oil. Sensors. 2023; 23(24):9796. https://doi.org/10.3390/s23249796
Chicago/Turabian StyleElele, Ugochukwu, Azam Nekahi, Arshad Arshad, Kate McAulay, and Issouf Fofana. 2023. "Sensitivity Analysis of Intensity-Modulated Plastic Optical Fiber Sensors for Effective Aging Detection in Rapeseed Transformer Oil" Sensors 23, no. 24: 9796. https://doi.org/10.3390/s23249796
APA StyleElele, U., Nekahi, A., Arshad, A., McAulay, K., & Fofana, I. (2023). Sensitivity Analysis of Intensity-Modulated Plastic Optical Fiber Sensors for Effective Aging Detection in Rapeseed Transformer Oil. Sensors, 23(24), 9796. https://doi.org/10.3390/s23249796