Next Article in Journal
First Identification of Amphidinols from Mexican Strains and New Analogs
Previous Article in Journal
Metabolome-Based Classification of Snake Venoms by Bioinformatic Tools
Previous Article in Special Issue
Introduction to This Special Issue of Toxins: Application of Novel Methods for Mycotoxin Analysis
 
 
Search for Articles:
Title / Keyword
Author / Affiliation / Email
Journal
Article Type
 
 
Advanced Search
 
Section
Special Issue
Volume
Issue
Number
Page
 
Journals
Toxins
Volume 15
Issue 2
10.3390/toxins15020162
toxins-logo
Submit to this Journal Review for this Journal Propose a Special Issue
► Article Menu

Article Menu

share Share announcement Help format_quote Cite question_answer Discuss in SciProfiles thumb_up
...
Endorse textsms
...
Comment
Correction to Toxins 2021, 13(12), 883.
first_page
settings
Order Article Reprints
Font Type:
Arial Georgia Verdana
Font Size:
Aa Aa Aa
Line Spacing:
Column Width:
Background:
Correction

Correction: Addante-Moya et al. Assessment of the Optimum Linker Tethering Site of Alternariol Haptens for Antibody Generation and Immunoassay Development. Toxins 2021, 13, 883

by
Luis G. Addante-Moya
1,
Antonio Abad-Somovilla
1,
Antonio Abad-Fuentes
2,
Consuelo Agulló
1 and
Josep V. Mercader
2,*
1
Department of Organic Chemistry, University of Valencia, Doctor Moliner 50, 46100 Burjassot, Valencia, Spain
2
Spanish Council for Scientific Research, Institute of Agrochemistry and Food Technology, Agustí Escardino 7, 46980 Paterna, Valencia, Spain
*
Author to whom correspondence should be addressed.
Toxins 2023, 15(2), 162; https://doi.org/10.3390/toxins15020162
Submission received: 9 February 2023 / Accepted: 9 February 2023 / Published: 16 February 2023
(This article belongs to the Special Issue Application of Novel Methods for Mycotoxins Analysis)
Browse Figures
Versions Notes

Misplace of Schemes

In the original publication [1], Scheme 1 and Scheme 2 are misplaced due to mistakes in the publication process. Scheme 1 should be placed in the position of Scheme 2 and vice versa.
The correct schemes should be as follows:
Toxins 15 00162 sch001 550
Scheme 1. Synthesis of ALa-NHS ester. Reagents and conditions: (a) Br(CH2)4CO2CH3, K2CO3, KI, Bu4NBr, acetone, reflux, 16 h, 75% of 3. (b) Tf2O, pyridine, 0 °C to rt, 20 h, 91%. (c) i. n-BuLi, THF, −78 °C, 40 min; ii. B(OiPr)3, −78 °C to 0 °C, 1.5 h, 93%. (d) Pd(PPh3)4, K2CO3, DMF, 93 °C, 24 h, 75%. (e) i. HCl, MeOH, rt, 22 h; ii. TFA, CH2Cl2, rt, 20 h, 97%. (f) Lipase acrylic resin, THF-PB 100 mM, rt, 20 h, 93%. (g) EDC·HCl, NHS, DMF, rt, overnight, 99% of crude product.
Scheme 1. Synthesis of ALa-NHS ester. Reagents and conditions: (a) Br(CH2)4CO2CH3, K2CO3, KI, Bu4NBr, acetone, reflux, 16 h, 75% of 3. (b) Tf2O, pyridine, 0 °C to rt, 20 h, 91%. (c) i. n-BuLi, THF, −78 °C, 40 min; ii. B(OiPr)3, −78 °C to 0 °C, 1.5 h, 93%. (d) Pd(PPh3)4, K2CO3, DMF, 93 °C, 24 h, 75%. (e) i. HCl, MeOH, rt, 22 h; ii. TFA, CH2Cl2, rt, 20 h, 97%. (f) Lipase acrylic resin, THF-PB 100 mM, rt, 20 h, 93%. (g) EDC·HCl, NHS, DMF, rt, overnight, 99% of crude product.
Toxins 15 00162 sch001
Toxins 15 00162 sch002 550
Scheme 2. Synthesis of ALb-NHS ester. Reagents and conditions: (a) Pd(PPh3)4, K2CO3, DMF, 95 °C, 19 h, 77%. (b) NaH2PO4·H2O, NaClO2, tBuOH-H2O (5:1), rt, 5 h, 96%. (c) iPrOH, THF, conc HCl, 55 °C, 24 h, 98%. (d) Br(CH2)4CO2CH3, Cs2CO3, DMF, 94%. (e) Lipase acrylic resin, THF-PB 100 mM, rt, 20 h, 99%. (f) EDC·HCl, NHS, DMF, rt, overnight. (g) 5% Pd/C, acetone, H2 (1.5 atm), rt, 19 h, 95% of crude product from 14.
Scheme 2. Synthesis of ALb-NHS ester. Reagents and conditions: (a) Pd(PPh3)4, K2CO3, DMF, 95 °C, 19 h, 77%. (b) NaH2PO4·H2O, NaClO2, tBuOH-H2O (5:1), rt, 5 h, 96%. (c) iPrOH, THF, conc HCl, 55 °C, 24 h, 98%. (d) Br(CH2)4CO2CH3, Cs2CO3, DMF, 94%. (e) Lipase acrylic resin, THF-PB 100 mM, rt, 20 h, 99%. (f) EDC·HCl, NHS, DMF, rt, overnight. (g) 5% Pd/C, acetone, H2 (1.5 atm), rt, 19 h, 95% of crude product from 14.
Toxins 15 00162 sch002
The authors state that the scientific conclusions are unaffected. The original publication has also been updated.

Reference

  1. Addante-Moya, L.G.; Abad-Somovilla, A.; Abad-Fuentes, A.; Agulló, C.; Mercader, J.V. Assessment of the Optimum Linker Tethering Site of Alternariol Haptens for Antibody Generation and Immunoassay Development. Toxins 2021, 13, 883. [Google Scholar] [CrossRef]
Disclaimer/Publisher’s Note: The statements, opinions and data contained in all publications are solely those of the individual author(s) and contributor(s) and not of MDPI and/or the editor(s). MDPI and/or the editor(s) disclaim responsibility for any injury to people or property resulting from any ideas, methods, instructions or products referred to in the content.

Share and Cite

MDPI and ACS Style

Addante-Moya, L.G.; Abad-Somovilla, A.; Abad-Fuentes, A.; Agulló, C.; Mercader, J.V. Correction: Addante-Moya et al. Assessment of the Optimum Linker Tethering Site of Alternariol Haptens for Antibody Generation and Immunoassay Development. Toxins 2021, 13, 883. Toxins 2023, 15, 162. https://doi.org/10.3390/toxins15020162

AMA Style

Addante-Moya LG, Abad-Somovilla A, Abad-Fuentes A, Agulló C, Mercader JV. Correction: Addante-Moya et al. Assessment of the Optimum Linker Tethering Site of Alternariol Haptens for Antibody Generation and Immunoassay Development. Toxins 2021, 13, 883. Toxins. 2023; 15(2):162. https://doi.org/10.3390/toxins15020162

Chicago/Turabian Style

Addante-Moya, Luis G., Antonio Abad-Somovilla, Antonio Abad-Fuentes, Consuelo Agulló, and Josep V. Mercader. 2023. "Correction: Addante-Moya et al. Assessment of the Optimum Linker Tethering Site of Alternariol Haptens for Antibody Generation and Immunoassay Development. Toxins 2021, 13, 883" Toxins 15, no. 2: 162. https://doi.org/10.3390/toxins15020162

APA Style

Addante-Moya, L. G., Abad-Somovilla, A., Abad-Fuentes, A., Agulló, C., & Mercader, J. V. (2023). Correction: Addante-Moya et al. Assessment of the Optimum Linker Tethering Site of Alternariol Haptens for Antibody Generation and Immunoassay Development. Toxins 2021, 13, 883. Toxins, 15(2), 162. https://doi.org/10.3390/toxins15020162

Note that from the first issue of 2016, this journal uses article numbers instead of page numbers. See further details here.

Article Metrics

Back to TopTop