1. Introduction
Engineered lattice structures have been of keen interest to the metal additive manufacturing (AM) research community for many years. They have been used to reduce weight in aerospace applications [
1], provide porous in-growth surfaces in bone implants [
2], and reduce the amount of material and time needed to fabricate parts [
3]. Lattice structures used in these applications are typically constructed as three-dimensional (3D) arrays of a repeating unit cell geometry, or “building block”, such as those seen in
Figure 1.
Figure 1a–d show four unit cells that form open-cell lattices when patterned into 3D arrays.
Figure 1e–g show three unit cells that form closed-cell lattices when patterned into 3D arrays. Lastly,
Figure 1h–k show four types of triply periodic minimal surface (TMPS) unit cells that have unique properties in which the mean value of surface curvature is zero at all points.
From visual examination of the unit cells in
Figure 1, it is readily apparent that large arrays of repeating lattice unit cells cannot easily be fabricated via traditional manufacturing methods such as molding, casting, machining, or forming. The overwhelming majority of lattice structures are fabricated via additive manufacturing (AM) methods. Despite the growing use of metallic engineered lattice structures, industrial adoption of polymer lattice structures has been limited. This can be largely attributed to relatively poor mechanical properties of polymeric lattice structures compared with their metallic counterparts. The primary motivation for this research, therefore, is to improve mechanical performance of polymer engineered lattice structures using a novel AM technique with carbon fiber composite feedstock material.
One potential way to enhance mechanical properties of polymeric lattice structures is to consider use of carbon fiber reinforced polymer matrix (CFPM) composite materials. CFPM’s are increasingly being specified in the transportation industry as lighter weight replacements for some metallic materials. Weight reduction in transportation applications improves energy efficiency, reduces fuel consumption, and reduces CO2 emissions.
Although most research involving engineered lattices use AM to fabricate the structures, one of the simplest ways to construct engineered lattices is to cut 2D pieces from sheet material, and to then assemble those pieces into 3D structures. This is analogous to how 3D puzzles are constructed. For example, Jenett et al. [
4], Xu et al. [
5], and Dong and Wadley [
6] each describe manual assembly approaches to fabricating cellular structures. These research groups use low cost methods such as waterjet machining, laser cutting, or CNC machining, to cut 2D patterns from sheet-based material. The 2D shapes are manually assembled with interlocking joints, and then bonded using adhesives, brazing, sintering, or similar methods. The significant advantages of this approach are its simplicity and relatively low cost. Dong and Wadley’s work is also noteworthy in that it demonstrated the ability to cut carbon fiber composite beams from sheet material, thus providing excellent strength and stiffness in the assembled lattice structures. These methods show excellent potential for use in low volume production. However, drawbacks include high labor content as well as potentially high material wastage (scrap) when cutting 2D components out of expensive carbon fiber composite sheets/plates. Furthermore, they are not well suited for producing lattice structures out of non-cubic shapes, such as the dome structure shown in
Figure 2a.
Figure 2b shows a conformal lattice structure in which the lattice unit cell bounding boxes are not cubic, as shown in
Figure 1, but rather they are morphed to conform (flow) with the shape of the non-planar surfaces they are bound by.
As previously mentioned, the most widely used polymer AM processes to fabricate lattice structures fall into four categories. Vat polymerization methods, such as stereolithography (SLA), uses a scanning laser or projected image to photopolymerize selected regions of a layer of a (typically) acrylate or urethane photopolymer resin. Then, a new layer of resin is spread onto the first layer, and a second layer pattern is cured. The process repeats itself one layer on top of another until the part is complete. Dar et al. [
7] used the projection SLA method to fabricate BCC lattice structures, and Ge et al. [
8] present a review of research using a micro-projection SLA with resolution capabilities down to 2 μm/pixel. Vat polymerization can be used to fabricate micro and even nano-scale lattice structures with incredible feature resolutions [
9]. Li and Shen [
10] present a very interesting approach to designing 3D printed lattice structures in which the beam thickness in face-centered cubic (FCC) unit cells was locally increased or decreased based on FEA simulations. In areas with high stress, the beam thicknesses were increased to strengthen those regions. In low stress areas, the beam thickness were decreased in order to reduce mass. This resulted in heterogeneous lattice structures. The design method was validated using the stereolithography 3D printing process and 3-point bend tests. Although this research study did not use composite polymer matrix composite material, the design method would be amenable to use with the Axial Lattice Extrusion 3D printing technique described in this paper. The potential combinations are described in the Future Research section of the paper.
Although vat polymerization is extremely well suited for nano/micro-scale lattice structures, they are not as well suited for producing physically large lattice structures needed for transportation applications. Large vats of photopolymers would be extremely costly, and would be difficult to shield from oxidation and unwanted UV curing from stray light each time the machine is opened. Postprocessing of these parts also requires submersion and rinsing in solvent baths to remove uncured resin from the surfaces of the parts. That would be a challenge for extremely large parts. Lastly, the need to remove uncured resin from the beams of lattice structures would be problematic for parts whose surfaces are made of solid skins that encapsulate the internal lattice structure (i.e., removal of trapped uncured resin would be a challenge).
The second mainstream polymer AM process that may be used to fabricate lattice structures is material jetting. Polymer material jetting is typically done via layerwise inkjet printing and UV curing of acrylate or epoxy photopolymers. AM via inkjet material deposition is intriguing in the sense that (1) hundreds of parallel nozzles jetting material at typically 2 kHz or greater frequencies allows parts to be built at higher speeds than most other polymer AM processes, and (2) the use of multiple inkjet heads allows multiple materials with different properties to be deposited. In the same way that cyan, yellow, and magenta inks can be combined in different proportions to produce desired pixel colors in document printing, precise control over Shore hardness within a 3D printed part can be achieved by blending rigid and soft photopolymers in the desired proportion at each voxel (3D pixel) location via inkjet printing. For example, Kozior and Kundera [
11] used a Stratasys Eden material jetting machine to print 13 mm × 13 mm × 6.3 mm and 26 mm × 26 mm × 12.6 mm cellular structures using blends of rigid and soft materials. The samples were compressed in order to assess stress relaxation of the blended material structures as a function of time.
As is the case with vat polymerization, using material jetting methods to produce large scale high strength lattice structures is a challenge. In order for 3D inkjet printing to work with lattice structures, the void space within the lattice structure must be completely filled with a sacrificial support material that is removed after printing is complete. This support structure must be removed via post-processing, and that is exceedingly difficult if the parts have solid skins (surfaces) on them. Furthermore, the photopolymers must have very low viscosity (typically <10 cP) and precisely controlled surface tension (typically ~30 dynes/cm) to be compatible with inkjet printing. These photopolymers are very costly on a volumetric basis, which makes fabrication of large parts impractical. For these reasons, photopolymer material jetting has not been widely studied for production of polymer lattice structures.
Polymer powder bed fusion (PPBF) is the third mainstream AM process to be considered for making polymer lattice structures. With PPBF, a layer of thermoplastic powder is spread out, and radiant heating is used to preheat the powder bed to prevent thermal distortion during processing. A laser is then selectively scanned over regions of the powder bed to be melted. A fresh layer of powder is spread on top of the first layer, and the process is repeated layer-by-layer until the part is complete. The process is largely limited to for with semi-crystalline thermoplastics due to the need for powder scanned by the laser to rapidly melt, flow out and merge with previously densified material, and then rapidly solidify. The melt viscosities of amorphous thermoplastics are generally too high to flow out and properly densify for use with SLS [
12]. Polyamide (PA12) is by far the most commonly used thermoplastic with polymer PBF.
Cobian et al. [
13] printed small 30 mm × 15 mm × 15 mm “octet like” PA-12 lattice cubes with PPBF. Tension, compression and nanoindentation testing was performed on the samples. The authors concluded that the PPBF lattice structures were highly anisotropic, and that load direction was an important consideration when designing structures. Jin et al. [
14] propose a non-uniform lattice design approach in which the diameters of individual struts can be thickened where needed to better withstand expected mechanical loading using a topology optimization approach. The proposed method was demonstrated using PA-12 with a PPBF machine. Neither of these papers used fiber reinforced feedstock material, and both used relatively small sample sizes.
Despite the advantages of PPBF, commercially available machines are generally limited to modest build volumes on the order of 700 mm × 350 mm × 350 mm. This limits their utility for producing large-scale lattice structures. One reason for this is the need to preheat the powder bed to reduce/prevent thermal distortion of the part. Unused powder from each print job goes through heating and cooling cycles that significantly degrade the powder’s material properties. Unused powder can be blended with virgin powder, however, repeated thermal cycles will adversely affect mechanical properties. It is noted that metallic PBF processes (e.g., laser or electron beam PBF) have been the dominant method used to produce metallic lattice structures to date [
15,
16,
17,
18]. Aluminum and titanium alloys most typically used to produce these lattices have densities of ~2.7 and 4.2 g/cm
3, respectively. Likewise, the cost of their powders are in the
$100/kg and
$275/kg range, respectively. By way of comparison, carbon fiber composite feedstock materials of interest in this study have densities of ~1.2 g/cm
3 and prices of ~50/kg (exact values depend on the specific feedstock of course). Give the 2X–4X higher density and 2X–5X higher prices of metal powders compared with carbon fiber polymer matrix composite feedstocks, the aim of this paper is to explore lower cost and lighter weight polymer composite lattice fabrication. Metal PBF of lattice structures is therefore not covered any further here.
By far the largest category of mainstream polymer AM processes is fused filament fabrication (FFF). With this process, thermoplastic filament is extruded through a nozzle onto a moving substrate to lay down material in a desired geometric pattern. The process is repeated layer-by-layer until the 3D part is completed. Unlike most other polymer AM processes, FFF is very well suited for the fabrication of large parts, such as those of interest in this work. For example, Post et al. [
19] used FFF to fabricate a full-scale boat hull that was more than 10 m long. Naboni et al. [
20] used a similar process to fabricate a pavilion structure covering an area of 36 m
2. Another advantage of FFF is that low cost commodity thermoplastic materials used in conventional plastic injection molding can be used. These include thermoplastic materials reinforced with chopped carbon fibers to enhance mechanical properties.
Despite the advantages of FFF, the use of FFF to produce lattice structures for practical applications has been severely limited. This can be largely attributed to the relatively poor interlayer bonding associated with FFF. Unlike metal AM processes in which interlayer metallic bonding is generally quite good, interlayer bonding in FFF processes is known to be poor [
21]. This poor bonding can be explained using reptation theory which is often used to characterize bond strength between polymer interfaces [
22]. This theory holds that the bond strength at an interface (i.e., interfaces between printed layers in an FFF part) is heavily influenced by (1) the temperature of the polymer(s) when the interface is created, (2) the time that the polymers are maintained above the glass transition temperature, and (3) the amount of pressure applied at the interface during processing. This unfortunately results in conflicting objectives for FFF when large scale parts are to be produced. Unlike injection molding, thermoplastic material extruded from a nozzle is not constrained within a cavity. It is therefore difficult to apply high pressure during FFF to improve interlayer bonding. That leaves temperature and time as the primary controllable factors. If one chooses to 3D print at very low speeds and elevated temperature in order to produce high strength bonds between printed layers, the time needed to produce physically large parts becomes unacceptably long. If one increases print speed to reduce build times, then very poor interlayer bond strengths are to be expected.
These challenges are exacerbated when using FFF to print lattice structures.
Figure 3 illustrates a 3D lattice structure that is comprised of an array of vertical, horizontal, and diagonal cylindrical beams. When this structure is sliced into planar layers of material that get printed via conventional FFF, one can clearly see in the zoomed-in inset figure that each beam is produced as the result of dozens of vertically stacked small areas of extruded thermoplastic material. In the specific example shown in
Figure 3, the diagonal beams have a vertical height of 6 mm, and each printed layer has a thickness of 0.15 mm. Each beam therefore has 6 mm ÷ 0.15 mm = 40 polymer interfaces between printed layers. The structure as a whole in
Figure 3 has 5488 beams. Multiplying the number of beams by 40 polymer interfaces per beam, one arrives at 219,520 polymer interfaces in a small lattice cube that measures 84 mm × 84 mm × 84 mm. When this structure undergoes mechanical loading, there are literally hundreds of thousands of relatively weak polymer layer interfaces where cylindrical beams can fail. For parts at the scale of automotive, rail, marine, or airplane size scales, the number of polymer interfaces would be in the millions.
Although lattice structures printed via FFF have inherent difficulties stemming from hundreds of thousands or more weak interlayer bonds, there is considerable literature devoted to FFF lattice printing with different materials, geometries, and design methodologies. Abusabir et al. [
23] studied quasi-static and visco-elastic responses of simple cubic lattice structures 3D printed using polylactic acid (PLA) and acrylonitrile butadiene styrene (ABS) polymers. The authors concluded that plate lattice geometries were ideal for applications requiring high stiffness and creep resistance, whereas a shell-based cubic lattice structure was preferred for energy damping performance when quasi-static loading conditions are expected. All samples printed in the study used the traditional layerwise FFF printing process, and PLA and ABS polymers without fiber reinforcement were used.
Basurto-Vazquez et al. [
24] studied the energy absorbing performance of 3D printed polyethylene terephthalate glycol (PET-G) 2D cellular honeycomb structures fabricated using different orientations and infill densities. Compression testing revealed that 3D printing using 100% infill with an upright honeycomb orientation produced the best energy absorbing performance. All samples printed in this study used the traditional layerwise FFF printing process, and the PET-G material did not include fiber reinforcement.
Whereas the majority of engineered lattice publications deal with open-cell beam structures, Lin et al. [
25] studied wall-based lattice structures known as triply periodic minimal surfaces (TMPS). In recognition of the fact that numerical finite element analysis of large lattice structures can be computationally expensive, this study compared numerical FEA simulation results for a 3-point bend test with results predicted by purely analytical methods. The results differed by approximately 21%, which suggests that analytical methods may be suitable for initial design feasibility studies, but that it may not be accurate enough to guide final detailed design decisions.
None of the above mentioned FFF lattice papers made use of fiber reinforced composite feedstock material in an attempt to strength the structure. However, Cuan-Urquizo et al. [
26] examined the effect of 2D infill pattern geometry and infill density on bending stiffnesss using a wood PLA composite material. Specifically, 125 mm long × 25 mm wide × 6 mm thick three point bend test coupons were fabricated using hexagonal and star 2D infill patterns were printed with 20%, 30%, 40%, and 50% infill densities. The study concluded that the hexagonal infill pattern resulted in higher stiffness values with low infill percentages, whereas the star infill pattern resulted in higher stiffness values with higher infill percentages. Although this study used a composite material to produce FFF infills, the use of beam-based lattices was not considered.
Della Ripa et al. [
27] studied mechanical performance of several different lattice unit cell geometries that were printed using the traditional layerwise FFF process. This study used carbon fiber reinforced nylon as the feedstock material. The octet truss lattice geometry was found to have superior specific energy absorption (SEA) properties under quasi-static conditions. This paper also presented a simplified FEA simulation model that used 1D elements to quickly approximate behavior of the beams that make up the lattice structure. This publication used 3 × 3 × 3 unit cell arrays. It is common practice in the lattice design literature to use 5 or more unit cell replicates in each direction order to obtain reasonably accurate mechanical properties that are not skewed by behavior of unit cells at the outside (edge) faces of the cube [
28]. The paper does not describe the failure modes during testing in terms of where and how the structures failed.
Boursier Niutta et al. [
29] extended the Dell Ripa et al. study by focusing exclusively on the octet truss lattice structure. Small octet truss unit cell arrays having 2 × 2 × 2, 3 × 3 × 3, and 4 × 4 × 4 replicates were printed using the conventional FFF process. Specific energy absorption values for a range of unit cell sizes and beam diameters were studied. The study also presented a computationally efficient finite element simulation approach with satisfactory agreement between simulated and experimental results. This study used traditional layerwise FFF, and the number of unit cell replication along the X, Y, and Z axes (2, 3, or 4) would ideally be higher to avoid the previously mentioned edge effects.
One aspect off all of the recently published FFF lattice printing work reviewed above is that they all use traditional layerwise FFF that produces large numbers of weak interlayer bonds within each strut as illustrated in
Figure 3.
Figure 3 illustrates the conventional layer-by-layer FFF process by which a lattice structure would normally be printed. If it were possible to instead print each cylindrical beam as one smooth continuous extrusion, then all of the interlayer bonds within each beam would be eliminated. At the same time, it is well known that the mechanical properties of carbon fiber composites are strongly dependent upon the fiber orientation [
30]. For engineered lattice structures, the maximum bending stiffness and strength in tension would occur if the fibers could be aligned with the longitudinal axis of each cylindrical strut. It is well known that chopped fibers become strongly aligned as they exit the extrusion nozzle in the FFF process [
31,
32,
33]. Thus if the cylindrical beams were extruded in continuous move from the base of the strut to the tip of the strut, and if the extruded material contained chopped reinforcing fibers, then one would expect those fibers to be aligned with the axis of the strut. The remainder of this section explores these concepts that form the crux of this paper.
This paper seeks to explore the potential of FFF to produce high strength polymer composite lattice structures. The objective is to produce lattice beams that are smooth and continuous, and in which the fibers within each beam align with the longitudinal axis. In order to do this, the traditional layer-by-layer FFF fabrication approach is abandoned in favor of an Axial Lattice Extrusion (ALE) approach [
34]. With ALE, each vertical or diagonal strut within a lattice structure is produced in one single continuous upwards extrusion motion rather than being printed as a lamination of many small area patches. The process is illustrated in
Figure 4. First, the FFF extrusion nozzle starts at the base of the first beam (Point 1) and continuously extrudes in a diagonal upward motion to Point 2 (
Figure 4a) to extrude the first beam in one single movement. Material extrusion from the nozzle is stopped, and the extrusion head moves to the base of the second beam (Point 3 in
Figure 4b). Material is then extruded while the nozzle moves from Point 3 to Point 4 (
Figure 4b).
Figure 4c shows the 3rd and 4th struts on the bottom half of a simple unit cell after printing. To print the first strut in the top half of this unit cell, the extrusion head starts at Point 5 and extrudes continuously to Point 6 (
Figure 4d). The remaining three beams in the upper half of this unit cell are produced in similar fashion to produce a complete unit cell as seen in
Figure 4e. Finally,
Figure 4f shows the expected fiber alignment with each cylindrical beam. The orientation angles of the beams in
Figure 4e are provided as a convenience for the reader. For any size cube with a side length of
L, the angle (
) of any beam that connects opposing corners of the cube is:
In order to prevent the extruded material from sagging during the unsupported upwards motion, a gentle stream of air or nitrogen gas is blown onto the extruded beams to rapidly cool and solidify the extruded material. While
Figure 4 illustrates the ALE method for printing one unit cell, the process is readily repeated as many times as needed to print 3D repeating arrays of unit cells. The continuous extrusion movement that starts at the base of each beam and ends at the upper tip of each beam is ideal in the sense that (1) it produces a smooth beam that completely eliminates all weak interlayer bonds within the beam, and (2) the chopped fibers will theoretically align with the axis of the strut during extrusion, thus providing considerable tensile strength and bending stiffness.
Variations on the ALE deposition strategy have been explored by a very small number of researchers. Most published ALE related research has focused exclusively on printing just the exterior wireframe surface of an object via ALE [
35,
36].
Figure 5a shows a surface lattice where the surface of a 3D volumetric shape is covered with a lattice structure, but the inside is hollow. 3D printed surface lattices are motivated by the desire to quickly prototyping the shape of an object, however, they are not generally intended for structural applications. Of greater interest for this work is use of FFF to produce polymeric engineered truss lattice structures that occupy the full 3D volume of a part. A volumetric lattice is shown in
Figure 5b.
Among the published work, Liu et al. [
37] is one of the few to specifically describe a volumetric ALE deposition strategy using carbon fiber reinforced thermoplastic feedstock material. In this work, sandwich core panels were made using FFF to print one, two, and three layer pyramidal lattice structures that were then epoxied to the face sheets. PLA reinforced with continuous carbon fiber was the feedstock material. Quasi-static compression tests were performed using BCC lattice structures to assess performance as a function of length of the extruded beams. The maximum achieved compressive strength modulus values were 1.24 MPa and 27.70 MPa, respectively. The fact that this study used continuous carbon fiber reinforcement is quite noteworthy, although the researchers reported some complications with lattice printing.
Among the polymer AM processes that have been used to fabricate lattice structures, FFF stands out as the process that is best suited to produce large scale lattices needed for transportation applications that will most benefit from the high strength and stiffness to weight ratios. However, improvements are needed in the traditional layerwise FFF process to eliminate hundreds of thousands to millions of relatively weak polymer interfaces. The remainder of this paper is dedicated to a feasibility study on use of the ALE approach to produce octet truss lattice structures such that (1) the polymer interfaces within the beams are eliminated, and (2) fiber reinforcements are aligned with the axis of the beams. Finite element modeling that captures the highly orthotropic nature of the fiber reinforced lattice structures is of value for engineering design and analysis purposes, hence a modeling approach and experimental validation are also presented. Experimental testing is used to assess performance of the preliminary ALE fiber reinforced lattices and to guide recommendations for future research.