2.1. Test Specimen
The regular hexagon aluminum honeycomb structure is adopted. The hexagonal aluminum honeycomb structure is commonly made of 0.02–0.1 mm thick aluminum foil through bonding. There are two manufacturing methods, forming and stretching. Stretch method is suitable for industrial production due to the high efficiency, so it is widely used. The process flow of the stretch method to manufacture aluminum honeycomb structure include aluminum foil cleaning, node glue, solidification, slitting, stretch. The cleaning process mainly contain alkali wash, rinsing, phosphoric anodization, spray and drying. Then J-70 adhesive based on the epoxy resin is applied, which can inhibit corrosion. The gluing process is completed by a special gluing machine. After that, the coated aluminum foil needs to be folded to form a panel and then curing. The curing parameters are related to the selected adhesive, generally speaking, the pressure is 0.5 Mpa, the time is 3–5 min. After slitting and stretching forming, the honeycomb panel is formed.
The basis material of the aluminum honeycomb structure is 5052 aluminum alloy. The chemical composition is shown in
Table 1. The cell characteristics are as follows: the cell wall thickness
t is 0.06 mm with the length
l of 1.732 mm; cell structure characteristic size
d is 3 mm, as shown in
Figure 1. The wall thickness of the opposite cells in each cell structure is 0.12 mm due to the manufacturing method. The thickness of the aluminum honeycomb structure sample is 5 mm, and 3 samples were prepared for each test. The coordinate system of the aluminum honeycomb structure is shown in
Figure 2. The direction
x3 is the direction of the out-of-plane loading, and
x1 and
x2 are the directions of the in-plane loading.
2.2. The Special Measures of Split Hopkinson Pressure Bar (SHPB) Test Method and Verification
The SHPB method is widely used in dynamic compression tests for metal materials to obtain the dynamic mechanical properties. However, there are still many difficulties when it is applied to the honeycomb structure, especially at the high strain rate, which are mentioned before. The following special measures are taken to overcome the difficulties.
The actual impact area of the honeycomb structure is small compared to metallic materials due to the thin cell wall during the impact, which may cause the stress nonuniformity of the specimen and the divergence of the stress wave. The specimen of Φ32 is applied to reduce the stress nonuniformity and the divergence of the stress wave as well as the diameter of the incident bar is 37 mm. The specimen contains nine complete cells in the direction of diameter. Try to maintain the integrity of cells at the edge of the specimen during the processing.
The wave impedance of the honeycomb structure is lower than that of aluminum alloy bar which makes the weak signal in the transmission bar. The semiconductor strain gauge is applied on the transmission bar to acquire the nice waveform of the weak signal, which cannot be measured by the conventional resistance strain gauge. It is also more convenient than the adoption of the viscoelastic bar. The contact surface between the bar and the specimen is lubricated to reduce the friction between the end face of the specimen, the incident bar as well as the transmission bar.
The loads between the impact end and the support end of the specimen may be different due to the divergent oscillation of incident wave, resulting in poor stress uniformity inside the specimen. Therefore, the brass wafer is pasted at the impacted end of the incident bar to eliminate the unbalanced stress caused by the divergence of the stress wave.
The short specimen and long impact bar are employed to make the stress wave passing through at least 3–4 reflections in the specimen, realizing the homogenization of the stress in the specimen.
The measurements based on the SHPB method are shown in
Figure 3.
The length of the impact bar is 0.6 m, and those of the incident and transmission bars are 2 m. The strain gauges are pasted at 0.85 m from the impact end of the incident bar and the middle of transmission bar respectively, to obtain the strain curves of the incident and transmission bars in the loading process, and then the stress–strain relationship of the specimens can be obtained. The size of the specimen of Φ32 × 5 mm is adopted in the dynamic compression tests.
The measurements based on the SHPB method are verified by the direct impact tests of impact end and support end which are modified from the SHPB test. The stress responses of the impact end and the support end of the aluminum honeycomb structure are obtained, respectively, by the twice impact method, so as to verify the effectiveness of the measurements of SHPB test method.
The direct impact tests of the support end are shown in
Figure 4. The aluminum honeycomb structure specimen is contacted with the transmission bar in the SHPB test system, and the semiconductor strain gauge is pasted on the transmission bar. The distance between strain gauge and the impact end of the bar is 0.85 m. The incident bar is removed, and a long elastic impact bar is adopted to impact the specimen at a certain velocity directly. It is called test 1.
The direct impact tests of the impact end are shown in
Figure 5. The specimen is contacted with the end of the impact bar, then the specimen with the impact bar hit the transmission bar at a certain velocity. The strain is measured by the semiconductor strain gauge on the transmission bar, and then we can obtain the stress response through calculation. It is called test 2.
The pictures of the direct impact tests are shown in
Figure 6 and
Figure 7 respectively.
The strain-time curve of the transmission bar is obtained by the strain gauge measurement in the direct impact tests of both impact end and support end. The transmission bar is made of hard aluminum alloy, which causes elastic deformation during the impact. The stress of the transmission bar can be calculated as
The force on the contact surface between the honeycomb structure and the transmission bar can be calculated as
The stress of the honeycomb structure can be calculated as
where
is the stress of the honeycomb structure,
is the sectional area of the transmission bar,
is the initial macroscopic sectional area of the honeycomb structure,
is the elasticity modulus of the transmission bar, and
is the strain-time curve of the transmission bar. It is noticed that the sectional area of the honeycomb structure
varies during the impact, so the stress of the honeycomb structure
is the nominal stress.
The SHPB test with measurements is conducted in order to compare the stress response of the direct impact test and SHPB test. It’s called test 3.
The impact velocity at high strain rate is adopted in the tests. The impact velocities of three tests are 13.83 m/s, 14.41 m/s and 13.85 m/s respectively. The results of the tests are shown in
Table 2, and the stress curve is shown in
Figure 8.
There is a time delay about the stresses compared to each test, as shown in
Figure 8. The time delay is caused by the distance between the impact end and the support end of the specimen. The time delay between the impact end and the support end is 0.02 ms.
There is not only a time delay between each test, but also a stress value difference. The equilibrium stress factor
R(
σ) of the specimen is defined as the ratio of the difference of the maximum and minimum mean nominal plateau stress to the average value. The equilibrium stress factor can measure the stress uniformity. The calculation formula is as follows
where
is the maximum mean nominal plateau stress of the three tests,
is the minimum mean nominal plateau stress of the three tests,
is the average value of
and
. In general, when
R(
σ) < 5%, it is considered the stress is uniform [
17]. The test results show that the stress factor
R(
σ) of three tests is 4.06%, which meets the requirement of stress uniformity in the specimen. It is verified that the special measures of SHPB method can be used in the dynamic compression test of the aluminum honeycomb structures at the high strain rate.
The dynamic compression tests of aluminum honeycomb structures at a strain rate of 1 × 103 s−1, 2 × 103 s−1 and 5 × 103 s−1 are carried out by adjusting the impact velocity of the impact bar to obtain the different strain rates. Three repetitions are performed at each strain rate.
2.4. Comparison at Different Strain Rates
The mean values of the dynamic compression test results (the strain rate of 1.3 × 10
3 s
−1, 2.0 × 10
3 s
−1, 4.6 × 10
3 s
−1, 6.67 × 10
−4) are fitted into the strain rate curves and the stress–strain curves at different strain rates, as shown in
Figure 16 and
Figure 17, respectively.
The compression of the quasi-static and the strain rate of 4.6 × 10
3 s
−1 both experience the elastic stage, the plateau stage and the densification stage. However, the strain rates of 1.3 × 10
3 s
−1 and 2.0 × 10
3 s
−1 only experience the elastic stage and the plateau stage, as shown in
Figure 17. It can be seen that there is no fluctuation at Quasi-static state, only one fluctuation at strain rate of 1.3 × 10
3, two fluctuations at a strain rate of 2.0 × 10
3, and three fluctuations at a strain rate of 4.6 × 10
3. The fluctuation appears in the plateau stage, which is because the cellular wall instability and buckling during the compression. It can be seen that the fluctuations increase with the strain rate increases.
The yield strength, the average plateau stress and the initial densification strain of the aluminum honeycomb structure at different strain rates are shown in
Table 6. The yield strength ratio at the strain rate of 2.0 × 10
3 s
−1 to the strain rate of 1.3 × 10
3 s
−1 is 1.03:1, while the average plateau stress ratio of them is 1.02:1. Additionally, the yield strength and the average plateau stress at the strain rate of 2.0×10
3 s
−1 and 1.3 × 10
3 s
−1 are both higher than that at the strain rate 6.67 × 10
−4. It is indicated that the aluminum honeycomb structure processes the stress hardening effect.
The yield strength ratios at the strain rate 4.6 × 103 s−1 to the strain rate 1.3 × 103 s−1 and 2.0 × 103 s−1 are 0.91:1 and 0.88:1, respectively, while the average plateau stress ratios of them are 0.95:1 and 0.93:1. It is indicated that the dynamic compression mechanical properties at the high strain rate of 4.6 × 103 s−1 process the stress softening effect.
The stress hardening effect and softening effect are both the combination of the characteristic of the honeycomb structure itself and the sealed gas effect. The characteristic of the honeycomb structure makes it exhibit higher stress in the dynamic compression tests at the high strain rate, however, the sealed gas effect plays the dominant role.
As the loading time is short in the dynamic compression tests at the high strain rate, the cell walls are not damaged, and the gas in the honeycomb cells can be approximately sealed, leading to the higher gas pressure. As the impact bar velocity increases, the yield strength and the plateau stress at the strain rate of 2.0 × 103 s−1 are higher than those at the strain rate of 1.3 × 103 s−1. However, as the impact bar velocity increases further, the cell walls seems partly damaged in the dynamic compression tests at the strain rate of 4.6 × 103 s−1 and the gas in the honeycomb cells can be partly sealed, leading to the lower gas pressure, so the yield strength and the plateau stress at the strain rate of 4.6 × 103 s−1 are lower than those at the strain rate of 1.3 × 103 s−1 and 2.0 × 103 s−1. Additionally, the gas flow out fully and the sealed gas effect is negligible in the process of the quasi-static compression, leading to the ambient gas pressure in the honeycomb cells, therefore the yield strength and the plateau stress at quasi-static are the lowest.
The initial densification strain is adopted as a material characteristic parameter to describe the crushability of the aluminum honeycomb structure in the maximum deformation of the plateau stage under the quasi-static and dynamic conditions. The dynamic compression at the strain rates of 1.3 × 103 s−1 and 2.0 × 103 s−1 does not reach the densification. The initial densification strain at the strain rate of 4.6 × 103 s−1 is smaller than that of the quasi-static stage, it is shown that the strain of the maximum deformation at a high strain rate is smaller than that at the quasi-static state.