As the fatigue test results include all influences from coupon microstructure to surface finish and loading parameters (i.e., stress or strain amplitudes, stress ratio, etc.), it is difficult to quantify the effect of each factor using empirical relationships. Therefore, in this section, the modified TMW model, Equations (3) and (4), will be used to separate individual effects in a stepwise manner. The discussion will address the fatigue performance of each type of material in the following sub-sections.
4.1. LB-PBF 17-4 PH
The conventional 17–4 PH is a martensitic stainless steel. Due to the high cooling rates during SLM, which are much faster than the critical cooling rate specified in the CCT diagram for 17–4 PH stainless steels, similar proportions of α’ and γ phases during martensitic transformation could form in LB-PBF 17–4 PH. Therefore, LB-PBF 17–4 PH samples might not be completely martensitic and contain retained austenite due to high solidification speeds during fabrication. The material chosen in this study has gone through the same heat treatment as its wrought counterpart, hoping to resume to the martensite phase as much as possible.
The fatigue test data of H1025 heat-treated wrought 17-4 PH, CA-H1025 heat-treated LB-PBF 17-4 PH and the HIPed and CA-H1025 heat-treated LB-PBF 17-4 PH stainless steel specimens are shown in
Table 3,
Table 4 and
Table 5, respectively. First, Equation (4) is used to analyze the fatigue data below the yield strength. Rearranging Equation (4), the fatigue strength for a given number of cycles can be expressed as:
where
is the stress amplitude.
Equation (5) can be used to perform linear regression analysis of the experimental data below the yield strength (<1100 MPa), as shown in
Figure 3. Especially, factors M and R
s can be obtained from the intercept and slope of the regression line:
The surface finish factor
and the microstructural factor
M for these material conditions are summarized in
Table 6.
Above the yield strength, as seen from
Table 3, plastic strain accumulates at nearly constant stress, causing the shortening of fatigue life. Therefore, the fatigue processes in this regime is LCF, and Equation (3) is used with
= 0.25. Note that the surface roughness effect for LCF is different from that for HCF. This is not totally unexpected as roughness may cause stress concentration under elastic loading, but it rather contributes directly to the formation of extrusions/intrusions during LCF when plasticity commences. The calculated fatigue lives are given in
Table 3,
Table 4 and
Table 5 and the curves are shown in
Figure 4 in comparison with the experimental data.
It can be inferred from
Table 6 results that the surface roughness in the range from 0.01 μm to 9 μm only causes about a factor of 3 variations in fatigue life. Normally, the surface finish factor
is less than 1; whereas surface enhancement treatment or residual stresses may cause it to be greater than 1, in the current context of the present model. It is noticed that in the case of CA-H1025-treated 17-4 PH with a machined surface,
= 1.5. It is uncertain whether this is due to a physical effect or simply an error in linear regression, as the data points are few.
On the other hand, the AM microstructure, perhaps together with roughness too, has a significant effect, reducing the fatigue strength, i.e., the fatigue endurance limit, to the maximum by a factor of 2 for 17-4 PH steel. Generally, the microstructural factor M reflects the effect of inclusions, as described by the inclusion theory of Eshelby [
16]. Shibata and Ono used Eshelby’s formulation to calculate the stress concentration factors of oblate inclusions with various aspect ratios and found that the stress concentration factor of a spherical void is 2.5 [
17]. Wu also used Eshelby’s theory to evaluate the effect of graphite inclusions (flake-like, vermicular or nodular) on the fatigue strength of cast irons [
18]. As porosities in AM materials are elongated in the horizontal direction, as depicted in
Figure 1, it should have a lesser stress concentration effect. The authors of the original experimental work examined the AM microstructure. They observed that the size of the pores in non-HIPed AM 17-4 PH was about 80 μm, and it was reduced to less than 20 μm after HIPing [
13]. Apparently, pores could not be fully eliminated due to the presence of pressurized entrapped argon gas inside the defects which could not escape or diffuse into the material. The effectiveness of the HIP process in reducing the porosities depends on the characteristics of the initial defects. In the case of large defects, the HIP process may not be effective [
19]. Pores may also appear on the as-built surface or be exposed by machining, which may or may not be reflected in the roughness measurement on selected areas. Nonetheless, the modified TMW model sheds light on the interpretation of the fatigue data and separates the convoluted microstructure-surface effects into what causes life scatter and what causes reduction in fatigue strength.
4.2. DMLS Ti6Al4V
Ti-6Al-4V is perhaps one of the most studied alloys in AM [
4,
5,
6,
14,
20,
21,
22,
23,
24]. Since titanium alloys are generally lightweight, bio-compatible and resistant to corrosion, it has a potential of wide applications in various industries with AM. The conventional wrought Ti-6Al-4V processes a dual-phase microstructure with equiaxed α + β grains or lamellar α + β colonies interspersed between nearly equiaxed α grains. The as-built SLM Ti-6Al-4V has a martensitic acicular α’ microstructure. Therefore, it has high static strength but poor ductility compared with cast or wrought Ti-6Al-4V [
4].
Due to the limited scope, the current analysis cannot cover all previous studies but can only take data from references [
14,
21]. The wrought material fatigue data are taken from reference [
21], which is considered as the baseline, and the behaviour is described by Equations (3) and (4) with
= 1 and M = 1, i.e., the baseline Equations (1) and (2), as given in
Table 7. The DMLS Ti6Al4V fatigue data are digitized from reference [
14]. The fatigue behaviours of AM Ti6Al4V are described by Equations (3) and (4), while
and M are evaluated in a similar way by Equations (5) and (6), and the values are given in
Table 8. The calculated curves are shown in
Figure 5, which are in good agreement with the experimental data.
The HIPed DMLS Ti6Al4V has a microstructure factor of 1.5, which is comparable to AM 17-4 PH, reasonably, with pores. However, the as-fabricated DMLS Ti6Al4V has a microstructural factor of 316, which is much larger than that raised by round pores. Therefore, it is suspected that this must be caused by LOF defects, which are usually larger and sharper than pores. The post-mortem fractographic examination in the original work revealed that fatigue crack initiation did start from surface defects, which propagated, linked up and prompted the final failure. Although mechanical polishing might remove some of the obvious defects on the surface, some remained due to the emergence of occasional voids from within the bulk during material removal. Treatment of DMLS specimens with either mechanical polishing or electropolishing produced negligible improvement in fatigue life. The surface finish factor has values ranging from 0.57 to 1, but it does not seem to correlate with the arithmetic average surface roughness, , for Ti6Al4V.
4.3. SLM AlSi10Mg
Aluminum alloys are also commonly used materials in AM. A recent review is provided by Aboulkhair et al. [
25]. Even though the number of Al alloys that are now processable by SLM with high fidelity is still limited, ongoing studies are expanding, aiming to widen the range. Most of the existing fatigue studies concentrate on SLM AlSi10Mg with its conventional counterpart Al 6061 [
14,
25,
26,
27,
28]. The microstructure of SLM AlSi10Mg typically consists of overlapping, segregated melt pools with distinct boundaries. The bulk material of SLM AlSi10Mg contains voids, which grow in both horizontal and vertical directions, but are more numerous in the material grown in the vertical orientation [
4,
14]. In addition, voids are more prevalent in the surface layers [
14,
27].
In the present study, the fatigue behaviours of wrought Al 6061, SLM AlSi10Mg in both horizontal and vertical orientations are analyzed using the modified TMW model, following the methods as described in the previous sections. The fatigue behaviours of SLM AlSi10Mg are described using Equations (3) and (4) with
and M values obtained using the method of Equations (5) and (6) as given in
Table 9. The calculated S-N curves are shown in
Figure 6 in comparison with the experimental data.
Interestingly, the horizontal AM microstructure factor (M = 1.7) is close to the other AM materials analyzed in this study. The vertical direction has a slightly higher microstructural factor (M = 2.08), but all within the range as caused by round ellipsoidal voids. The surface finish factor
of SLM AlSi10Mg is 0.756 in both directions, as the polished surface roughness is quite low with
= 1.5 μm. Fatigue crack nucleation in SLM AlSi10Mg was found to originate from pores, either internal or at the surface [
14].
Once the surface finish factor is determined, the TMW model can be used to assess the fatigue endurance limit per coupon such that a statistical distribution may be obtained as follows.
First, rearranging Equation (5), we have:
Then, Equation (8) is used to evaluate the coupon level
for every test, and the results are given in
Table 10 for wrought Al 6061 and SLM AlSi10Mg. This set of data can be turned into statistical distributions as shown in
Figure 7, and the distribution functions and parameters are given in
Table 11. The fatigue endurance limit of wrought Al 6061 can be represented by a log-normal distribution, but interestingly, that of the AM AlSi10Mg materials appear to be a normal distribution. During the AM process, the material’s microstructure is formed from powders under high energy input by a laser, which reasonably creates a new microstructure with a normal (symmetrical) distribution of properties. On the other hand, the wrought material has gone through complex thermomechanical processing, which may skew the property distribution. Other examples of the statistical distribution of properties can be found in metallic glasses [
29,
30]. It is beyond the scope of the current study to completely characterize the statistical distribution of processing-microstructure-property relationships for AM materials, but it is certainly an interesting point of future study. Nevertheless, once the AM material property distribution is determined, the design allowables can be evaluated for application of AM materials, as schematically shown in
Figure 8 [
7]. The TMW model can facilitate such evaluation by means of its simple analysis and fewer tests to determine the fatigue endurance limit, as opposed to the conventional method to conduct many material fatigue tests, up to 10
7 cycles.