Advances in Microstructural Characterization of Metallic Alloys

A special issue of Metals (ISSN 2075-4701). This special issue belongs to the section "Structural Integrity of Metals".

Deadline for manuscript submissions: closed (30 November 2022) | Viewed by 3874

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Department TEXMAT, Clausthal University of Technology and Helmholtz-Zentrum Geesthacht (HZG), Max-Planck-Str, D-21502 Geesthacht, Germany
Interests: materials characterization by X-rays; neutrons, synchrotron, and EBSD; instrumentation; texture, phase, and stress analysis; Mg, Al, and Ti alloys; industrial application
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Special Issue Information

Dear Colleagues,

Microstructural characterization is essential to understand the behavior of any kind of material. This Special Issue will focus on metallic alloys, because alloy development is an essential factor for obtaining new classes of materials for advanced applications in new transportation systems, new energy efficient systems, and prothesis development. Such a broad spectrum of requirements in advanced applications includes all groups of metallic alloys. Fe and steel business have a long tradition in alloying, but lightweight constructions need improved alloys. Lightweight alloys like Ti, Al, and Mg alloys have been heavily investigated in recent years, revealing their excellent properties.

Advanced methods to characterize a microstructure combine imaging methods with diffraction methods. The aim of all methods is to obtain detailed information of the 2D or, even better, 3D microstructure (grain size distribution; grain orientation distribution; precipitation distribution; 1D-, 2D-, and 3D-defect distribution; macro- and microstrain distribution; grain boundary information). Beside standard techniques, advanced in situ methods have been implemented for high-temperature studies and applied strain investigations, among others. These methods are based on optical microscopy, electron microscopy, X-ray diffraction, synchrotron radiation, and neutron radiation.

Indicative topics of the Special Issue scope are the following:

  • Electron backscatter diffraction (EBSD);
  • Synchrotron investigations (in situ diffraction, 3DXRD)
  • Time-resolved and classical X-ray diffraction
  • In situ neutron diffraction
  • Tomography
  • 2D microstructure
  • 3D microstructure
  • Defect density
  • Macro- and microstrain
  • Crystallographic texture (grain orientation distribution)
  • Metallic alloys (Fe, Cu, Ti, Al, Mg)

Special emphasis will be given to recent advances in the different techniques, to the characterization of produced parts regarding surface finish, dimensional accuracy, and/or mechanical properties, as well as to new applications of metallic materials.

Prof. Dr. Heinz-Günter Brokmeier
Guest Editor

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Keywords

  • EBSD
  • in situ diffraction
  • grain size distribution
  • grain boundaries
  • deformation of alloys
  • recovery of alloys
  • recrystallization of alloys
  • grain orientation distribution (crystallographic texture)
  • macrostrain and crack distribution
  • 3D-XRD

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Published Papers (2 papers)

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19 pages, 6356 KiB  
Article
The Nb-V-Ti-N-C System Microelements Coupling Precipitation Behavior and Its Effects on Properties in High Strength Naval Steel
by Lingtong Zhang, Bowei Zhang, Yanlin Wang, Zhihao Zheng, Xiaohua Chen, Xiaohua Zhou, Heinz-Günter Brokmeier, Zidong Wang and Hao Tang
Metals 2023, 13(1), 8; https://doi.org/10.3390/met13010008 - 20 Dec 2022
Cited by 5 | Viewed by 1608
Abstract
The Nb-V-Ti-N-C system microelements coupling precipitation behavior in high strength naval steel was thermodynamically analyzed. The effects of micron/nano particles on the microstructure, mechanical properties, and corrosion resistance were also studied by an in situ scanning electron microscopy (SEM) tensile test, transmission electron [...] Read more.
The Nb-V-Ti-N-C system microelements coupling precipitation behavior in high strength naval steel was thermodynamically analyzed. The effects of micron/nano particles on the microstructure, mechanical properties, and corrosion resistance were also studied by an in situ scanning electron microscopy (SEM) tensile test, transmission electron microscopy (TEM) analysis, and electrochemical polarization measurements. The results show that the solid solution amount of Nb, V, Ti, N, or C decreases in the steels as the temperature decreases. Carbonitrides begin to precipitate at 1506.39 °C in N1 steel, and the carbonitrides are nano-scale. Meanwhile, carbonitrides begin to precipitate at 1628.74 °C in N2 steel, which is 116.69 °C higher than the corresponding liquidus temperature of 1512.05 °C; carbonitrides with micron scale are formed in the metal melt. The tensile test revealed that with the increase in titanium content from 0.05% to 0.1%, the strength increases while the elongation decreases. The in situ SEM test results indicated that lower plasticity are associated with the carbonitrides of micron-scale, which are the micro crack sources under stress. Polarization test results indicated that pitting corrosion may easily occur at the abnormally large-sized (Nb, V, Ti)(C, N) carbonitrides. Full article
(This article belongs to the Special Issue Advances in Microstructural Characterization of Metallic Alloys)
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15 pages, 25936 KiB  
Article
Employment of Barkhausen Noise Technique for Assessment of Prestressing Bars Damage with Respect of Their Over-Stressing
by František Bahleda, Ivan Drevený, Martin Pitoňák, Miroslav Neslušan and Peter Koteš
Metals 2021, 11(5), 770; https://doi.org/10.3390/met11050770 - 7 May 2021
Cited by 4 | Viewed by 1640
Abstract
This paper investigates the potential of a non-destructive magnetic technique based on Barkhausen noise emission for the monitoring of prestressing bars with respect to their undesired over-stressing. Barkhausen noise signals are correlated with tensile stress, residual stresses, and microhardness measurements. It was found [...] Read more.
This paper investigates the potential of a non-destructive magnetic technique based on Barkhausen noise emission for the monitoring of prestressing bars with respect to their undesired over-stressing. Barkhausen noise signals are correlated with tensile stress, residual stresses, and microhardness measurements. It was found that prestressing bars exhibit strong magnetic anisotropy which becomes more pronounced along with the increasing degree of the bar’s over-stressing. Barkhausen noise emission becomes strongly attenuated in the direction of the tensile stress at the expense of the perpendicular direction. However, the Barkhausen noise emission in the direction of the tensile stress exhibits a continuous and remarkable decrease, whereas the Barkhausen noise steep increase for lower degrees of over-stressing is followed by early saturation for higher over-stressing. This study demonstrates that the Barkhausen noise technique is capable of distinguishing between the prestressing bars loaded below yielding, and those which are over-stressed. Full article
(This article belongs to the Special Issue Advances in Microstructural Characterization of Metallic Alloys)
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