Laser Welding of SLM-Manufactured Tubes Made of IN625 and IN718
Abstract
:1. Introduction
2. State-of-the-Art
3. Material and Methods
3.1. Materials
3.2. Experimental Procedure
3.3. Evaluation Tools
3.3.1. Residual Stress Measurements
3.3.2. Computed Tomography
3.3.3. Metallographic Investigations and Hardness Measurements
4. Results
4.1. Optical Evaluation of the Welding Results
4.2. Residual Stress Measurements
4.3. Computed Tomography (CT)
4.4. Metallographic Investigations and Hardness Measurements
5. Conclusions
- An optical inspection of the weld seams revealed no differences between the materials IN625 and IN718. However, a clear variation was found in the weld preparation. Post-processed tubes showed a shiny surface compared to raw (SLM edge) tubes, which showed an agglomeration of silicate-like inclusions on the top of the seam. It was not excluded that these impurities remained in the weld metal and led to a deterioration of weld seam quality. For this reason, a mechanical processing of the edges is recommended.
- The residual stresses were considered, as they often are a problem for additive manufactured components. For this reason, the residual stress values of the welded tubes, which were either with heat treatment or without heat treatment, were compared with the residual stresses values of the base material. The results show that there were some differences between the values for welded tubes and base material, especially for IN718. A heat treatment is therefore preferable. The weld edge preparation had no significant effect on the residual stress values.
- The most difficult part in welding the tubes consisted of the formation of pores and pore nests. As can be seen from the CT images, the quality in the seam circumference can be classified as good. Pores were mainly formed in the end crater area, in the area where a keyhole instability was observed. The problem of the weld defects, such as pores and cracks in the overlap area of the circumferential welds, was already known. For this reason, the tests were carried out with already adapted parameters and a laser power ramp. However, pores and cracks in the overlap area could not be completely avoided by any method tested. For further tests, it is necessary to reduce the pores in the critical overlap area so that the weld seams can reach the highest quality, Group B, reliably and reproducibly. Hence, the interaction between scanning parameters, such as frequency and amplitude, and other welding parameters have still to be clarified. Such investigations must be carried out considering thermophysical properties of melt, such as surface tension and viscosity, to allow the laser beam oscillation technique to be transferred to SLM tubes made from nickel-based alloys to eliminate the formation of pores [22,23].
- Further tests need to be made to improve the welding quality in the end crater area by defocusing the laser [24].
- It can be mentioned positively that there were no hot cracks in the weld seams, despite the materials IN625 and IN718 being often susceptible to them.
Author Contributions
Funding
Conflicts of Interest
References
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Alloy | Ni | Cr | Mo | Fe | Nb | Mn | Si | Al | Ti | C | Co | Ta | B | Cu |
---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
IN625 | bal. | 21.5 | 9 | 2.5 | 3.6 | 0.2 | 0.2 | 0.2 | 0.2 | 0.05 | ||||
IN718 | bal. | 18.5 | 3 | 16.3 | 5.1 | 0.1 | 0.4 | 0.5 | 1 | 0.05 | 0.3 | 2.5 | 0.004 | 0.2 |
Material | Type of Heat Treatment | Atmosphere (mbar) | Temperature (°C)/Heating Rate (K/min) | Holding Time (min) | Cooling Conditions |
---|---|---|---|---|---|
IN625 | solution annealing | <10–4 <10–4 | 1175/<25 | 60 60 | 40–60 K/min to 500 °C afterwards free cooling |
IN718 | 982/<25 |
Material | Heat Treatment Conditions | Tube Edge Quality | Number of Samples for the Material Combination | ||
---|---|---|---|---|---|
Heat Treatment (HT) | Without Heat Treatment (WOHT) | SLM Edges (SLME) | Mechanically Cut Edges (CE) | ||
IN625 | + | - | + | - | 3 |
IN625 | + | - | - | + | 3 |
IN625 | - | + | + | - | 3 |
IN625 | - | + | - | + | 3 |
IN718 | + | - | + | - | 3 |
IN718 | + | - | - | + | 3 |
IN718 | - | + | + | - | 3 |
IN718 | - | + | - | + | 3 |
Total number of samples | 24 |
Irregularities | Remarks | Valuation Groups with Limits for Irregularities | ||
---|---|---|---|---|
Low D | Middle C | High B | ||
Porosity and pores | Maximum size of a single pore in millimeters | 1.35 | 1.1 | 0.83 |
Maximum of the sum of the projection area of the irregularities in % | 6 | 2 | 0.7 | |
Pore nests and pore rows | Distance between individual pores in pore nests in millimeters | 0.68 | 1.35 | 1.35 |
Influenced weld seam length for pore nests in millimeters | 5.4 | 2.7 | 2.7 |
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Jokisch, T.; Marko, A.; Gook, S.; Üstündag, Ö.; Gumenyuk, A.; Rethmeier, M. Laser Welding of SLM-Manufactured Tubes Made of IN625 and IN718. Materials 2019, 12, 2967. https://doi.org/10.3390/ma12182967
Jokisch T, Marko A, Gook S, Üstündag Ö, Gumenyuk A, Rethmeier M. Laser Welding of SLM-Manufactured Tubes Made of IN625 and IN718. Materials. 2019; 12(18):2967. https://doi.org/10.3390/ma12182967
Chicago/Turabian StyleJokisch, Torsten, Angelina Marko, Sergej Gook, Ömer Üstündag, Andrey Gumenyuk, and Michael Rethmeier. 2019. "Laser Welding of SLM-Manufactured Tubes Made of IN625 and IN718" Materials 12, no. 18: 2967. https://doi.org/10.3390/ma12182967
APA StyleJokisch, T., Marko, A., Gook, S., Üstündag, Ö., Gumenyuk, A., & Rethmeier, M. (2019). Laser Welding of SLM-Manufactured Tubes Made of IN625 and IN718. Materials, 12(18), 2967. https://doi.org/10.3390/ma12182967