2.1.2. Selection of Corn Straw Contact Parameters
Corn straw from the experimental field of Jilin Agricultural University that was without obvious breakage or pest symptoms was selected as the test material. After the leaves of the selected straw were removed, only the culm portion was retained for the physical-mechanical test. The moisture content was 9.5 ± 1.5%. The density was determined via the drainage method, and the densities of the inner and outer skin of the straw were 185 kg/m3 and 614 kg/m3, respectively.
The Poisson’s ratio and modulus of elasticity of the straw, inner pulp, and outer skin were measured via uniaxial compression tests in a universal testing apparatus, as seen in
Figure 2 below. Each group underwent five repetitions of the single-factor test with a loading rate of 2 mm/min, and the final value was determined by averaging the results. Poisson’s ratio was calculated via Equation (1):
where
δ1 is the transverse deformation, mm;
δ2 is the axial deformation, mm;
W1 is the transverse dimension before compression, mm;
W2 is the transverse dimension after compression, mm;
L1 is the axial dimension before compression, mm; and
L2 is the axial dimension after compression, mm.
Finally, the inner pulp Poisson’s ratio of the straw was measured to be 0.26, and Poisson’s ratio for the outer skin was 0.10.
Equation (2) was used to get the modulus of elasticity:
where
F is the maximum bearing force, N;
L is the initial length, mm;
S is the sample cross-sectional area, mm; and ∆
L is the difference in length before and after sample compression, mm.
Finally, the moduli of elasticity of the inner pulp and outer skin of the straw were 48.44 MPa and 163.39 MPa, respectively.
Based on the experimental results and some parameters taken from references [
10,
18], the resulting material intrinsic parameters and contact parameters are shown in
Table 1.
Through the axial compression test of straw combined with the calibration method, the mechanical parameters of the parallel bonding model (PBM) of straw that were difficult to obtain experimentally, such as the normal critical stress, shear critical stress, normal stiffness coefficient, and shear stiffness coefficient, were calibrated, and the optimal parameter combinations were finally obtained.
For the simulation and simulation analysis, the Hertz‒Mindlin model with bonding particle contact was used, and the significance of the simulation parameters was analyzed via the PB test. Then, the levels of the test factors gradually approached the optimal ranges via the steepest ascent test. Finally, the BB test was carried out to derive the optimal combinations of the simulation parameters for the double-bonded bimodal distribution model of corn straw.
First, the literature was reviewed in order to choose the range of bonding parameter values [
10,
19,
20]; next, the range of bonding contact parameters was selected according to the moisture content of the corresponding straw, and the PB test was carried out to screen out the factors that were significant to the test results. The Design Expert 13 software was used, and the discrete element contact parameters of straw were taken as factors, denoted by A~D (the subscripts 1, 2, and 3 represent the contact parameters of the outer skin–outer skin, outer skin–inner pulp, and inner pulp–inner pulp, respectively), in which N~T are virtual parameters. The test values of each factor were used as the level values, and the response value was the compression force.
Table 2 provides the table of test parameter levels.
The loading speed of the axial simulation test plate was set to 2 mm/min, which was the same running speed as that of the mechanical test. A compression test simulation screenshot is shown in
Figure 3 below.
Figure 4 shows the comparison curve graphs of the compression test results of the simulation and the actual experiment. The figure shows that both have the same trend: approximate yielding occurs at the compression displacement near 2 mm. The experimental curve graph reveals that some yielding occurs at a compression displacement of 1.3 mm, while the yield is transitional rather than developmental; this is because parts of the stalk twist during compression, but the stalk may continue to compress when pressure is applied continuously.
The PB test consists of 20 groups of tests, for which the specific arrangements and results are listed in
Table 3 below.
Table 4 shows the significance analysis of the factors tested in the PB test, and the results of the test show that the model has a
p value of 0.0026 < 0.01, which is highly significant, making the model reliable; the coefficient of determination
R2 = 0.9454 indicates that the model is well correlated, has a good fit to the experimental data, and is applicable to 94.54% of the experimental data; the adjusted coefficient of determination, adjusted
R2adj = 0.8518, indicates that the model explains 85.18% of the response variable’s variability after accounting for the quantity of independent variables in the model;
p < 0.01 for A
3 and B
3, indicating that normal stiffness per unit area of inner pulp–inner pulp and shear stiffness per unit area of inner pulp–inner pulp have a highly important impact on the critical load; 0.01 <
p < 0.05 for A
1, indicating that normal stiffness per unit area of outer skin–outer skin has a significant effect on the critical load;
p > 0.05 for the other factors, suggesting that there is no discernible impact on the critical load.
Combined with
Figure 5, the Pareto chart for the PB test shows that factors A
1, A
3, and B
3 all exceeded the t = 2.36462 value and all had a favorable impact on the PB test response value, with A
3 being the most significant factor, indicating the direction of ascent in the steepest ascent test path.
In summary, the steepest ascent test was conducted for the three most significant factors—A
1, A
3, and B
3.
Table 5 displays the precise path configurations and outcomes. An examination of the results of the steepest ascent test, as shown in
Table 5, revealed that the critical load at the fifth set of test levels was 111.43 N, with the smallest relative error of 3.6% compared with the critical load of 115.64 N in the physical test. Here is observed the deviation between the measured value and the real value of the critical load on the corn straw. The relative error was calculated via Equation (3):
where
FP is the measured value of compressive force, N, and
FS is the simulation value of the compression force, N.
However, for the fifth group of tests as an endpoint and the critical load being smaller than the critical load of the actual experiment, the choice of high level should be adjusted. At this point, the sixth set of tests was added, and when A1 was 9.00 × 109 N/m3, A3 was 8.075 × 108 N/m3, B3 was 7.35 × 107 N/m3, and the critical load was 117.08 N, with a relative error of 1.2%. Therefore, Test 5 was selected as the center point in the follow-up test, and the factor levels of Test 4 and Test 6 were used as the low and high levels of the BB test, respectively, for the response surface test with three factors and three levels analysis.
Table 6 shows the BB test design and results. In this case, B
1 was 6.00 × 10
8 N/m
3, C
1 was 3.20 × 10
8 Pa, and D
1 was 3.00 × 10
7 Pa; A
2 was 6.00 × 10
8 N/m
3, B
2 was 4.00 × 10
8 N/m
3, C
2 was 3.00 × 10
7 Pa, and D
2 was 4.50 × 10
5 Pa; C
3 was 5.5 × 10
5 Pa, and D
3 was 3.50 × 10
5 Pa.
By fitting a quadratic multiple regression to the experimental results, the regression equation with the critical load as the response value was obtained as follows:
Y = 115.59 − 0.8025A
1 + 1.74A
3 + 1.45A
3 − 3.39A
1A
3 + 2.35A
1B
3 − 0.4175A
3B
3 − 2.17A
12 − 3.53A
32 − 3.75B
32. The coefficient of determination is
R2 = 0.9782, the adjusted coefficient of determination adjusted
R2adj = 0.9502, and the coefficient of variation is C.V. = 0.8196%. The regression equation indicated that the model fit was high enough to explain 95.02% of the variability in the response values, so ANOVA was performed on the BB test, the results of which are shown in
Table 7. The model has
p < 0.01, indicating that the model is highly significant and can reflect the connection between response values and factors—whereas the misfit term is not significant (
p > 0.05)—and that there is no significant misfit problem. The primary factors A
3 and B
3 have highly significant effects on the critical loads, and the effect of A
1 is significant. The effect of A
3B
3 is negligible, but the interaction terms A
1A
3 and A
1B
3 are considerable, and the effects of secondary terms A
12, A
32, and B
32 are highly significant. The effects of the factors on the response values did not have a simple linear relationship in the order of A
1 < B
3 < A
3.The regression equation was used to predict the compression force for each bonding parameter condition, and the relationship between the physical and simulation tests of the model was plotted (
Figure 6), as were the contour maps (
Figure 7). Based on the correlation between the expected and experimental values (
Figure 6), the distribution of the data points was close to the 45° fitting line and was more concentrated, which indicated that the model fit better and was more accurate in terms of prediction, and thus that it could be used for predicting and analyzing the compression force of corn straw. The contour maps show the trends and interactions of the effects of the factors, as well as the extent of the experiment conducted. The response variable that reached the optimal value appears in the red region. Combined with the BB test analysis of each optimal parameter value, A
1 was 8.20 × 10
9 N/m
3, A
3 was 6.81 × 10
8 N/m
3, and B
3 was 6.34 × 10
7 N/m
3.
In addition, the contact radius of the Hertz‒Mindlin bonding contact mechanics model is generally 1.2‒2 times the physical radius of the particles [
19]. To avoid bonding between non-neighboring particles or the instability of bonds formed by neighboring particles, many preliminary experiments concluded that the particles’ interaction radius was set to 1.2 times their own radius, which not only had a better simulation effect but also enabled the corn straw model to have certain flexible characteristics. Therefore, the outer skin particles had a contact radius of 0.9 mm, the inner pulp big particles had a contact radius of 1.2 mm, and the inner pulp small particles had a contact radius of 0.6 mm. The bonding radius and the contact radius were taken to be the same value, where the physical radius of dissimilar particles was taken as 1.2 times the center value, and the outer skin particle–inner pulp large particle bonding radius was 1.05 mm. The outer skin particle–inner pulp small particle bonding radius was 0.75 mm, and the inner pulp large particle–inner pulp small particle bonding radius was 0.9 mm.