Non-destructive Characterization and Processing of Composite Materials, Volume II

A special issue of Journal of Composites Science (ISSN 2504-477X). This special issue belongs to the section "Composites Modelling and Characterization".

Deadline for manuscript submissions: closed (30 September 2023) | Viewed by 4474

Special Issue Editor

Special Issue Information

Dear Colleagues,

This Special Issue aims to provide a good forum for scientists and engineers to share and discuss their pioneering original findings or insightful reviews on the characterization of composite materials. Reports on non-destructive characterization research towards process enhancement and the development/application of an advanced characterization method are particularly welcome.

The proper characterization of heterogeneous composite materials is still a challenging task, since the majority of characterization methods often require the size reduction and dissolution of a material that average the whole material and could overlook potential issues associated with spatially heterogeneous materials and values associated with fine grains (e.g., [1]).

Some potential contributions are listed below under “Topics”. One of them can be the characterization of industrial wastes for understanding the spatial distribution and liberation/association of key components in order to develop a recycling flowsheet. This correlation was found to be useful in many different respects, while there remain so many research gaps that have been identified. At the same time, better understanding heterogeneous composite materials is of great importance from scientific and engineering points of view, since the processing and production/application of composite materials are vital of our modern society, including raw materials (e.g., complex ores) and advanced technologies (e.g., batteries, printed circuit boards, [2–5]).

References

[1] A. Otsuki, Y. Chen, Y. Zhao, 2014. J. Soc. Mat. Eng. Res. 20(2) 126-135.

[2] Otsuki, A.; Gonçalves, P.P.; Stieghorst, C.; Révay, Z. Non-Destructive Characterization of Mechanically Processed Waste Printed Circuit Boards: X-ray Fluorescence Spectroscopy and Prompt Gamma Activation Analysis. J. Compos. Sci. 2019, 3, 54.

[3] Otsuki, A.; Pereira Gonçalves, P.; Leroy, E. Selective Milling and Elemental Assay of Printed Circuit Board Particles for Their Recycling Purpose. Metals 2019, 9, 899.

[4] Pereira Gonçalves, P.; Otsuki, A. Determination of Liberation Degree of Mechanically Processed Waste Printed Circuit Boards by Using the Digital Microscope and SEM-EDS Analysis. Electronics 2019, 8, 1202.

[5] Otsuki, A.; De La Mensbruge, L.; King, A.; Serranti, S.; Fiore, L.; Bonifazi, G. Non-destructive liberation analysis of mechanically processed waste printed circuits boards, Waste Management, 2020, 102, 510-519.

Topics

- Characterization

  • In-situ measurement (e.g., rheo-SANS, rheo-SAXS, rheo-NMR)
  • Neutrons, X-rays
  • Operando measurement
  • Imaging (e.g., SEM, TEM, tomography/radiography)
  • Surface analysis (e.g., AFM, STM, XPS, XAFS, reflectometry, mass spectrometry)
  • Suspension rheology
  • Physical/physico-chemical properties (e.g., particle surface charge, particle size, wetting, specific surface area, porosity)

- Physical chemistry

  • Heterogeneity
  • Concentrated colloidal suspension
  • Colloidal forces (e.g., DLVO forces, non-DLVO forces)
  • Chemical environment (e.g., salt/electrolyte, surfactant, pH)

- Process and functional materials

  • Industrial wastes
  • Complex ores
  • Mechanical processes (e.g., thickening/sedimentation, filtration, agitation/mixing)
  • Separation (e.g., flotation, magnetic separation)
  • Functional material synthesis and its characterization

- Fluid dynamics and applied mechanics

  • Particle-laden flow
  • Flow diagnosis
  • Flow visualization (e.g., MRI velocimetry)
  • Flow behavior under external field application (e.g., mechanical agitation, electric field application)
  • Non-Newtonian fluid
  • Complex fluid

Thank you very much!

Dr. Akira Otsuki
Guest Editor

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Keywords

  • physical chemistry
  • process and functional materials
  • flow dynamics
  • applied mechanics

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Published Papers (3 papers)

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Research

23 pages, 911 KiB  
Article
Concrete Compressive Strength Prediction Using Combined Non-Destructive Methods: A Calibration Procedure Using Preexisting Conversion Models Based on Gaussian Process Regression
by Giovanni Angiulli, Salvatore Calcagno, Fabio La Foresta and Mario Versaci
J. Compos. Sci. 2024, 8(8), 300; https://doi.org/10.3390/jcs8080300 - 1 Aug 2024
Viewed by 677
Abstract
Non-destructive testing (NDT) techniques are crucial in making informed decisions about reconstructing or repairing building structures. The SonReb method, a combination of the rebound hammer (RH) and the ultrasonic pulse velocity (UPV) tests, is widely used for this purpose. To evaluate the compressive [...] Read more.
Non-destructive testing (NDT) techniques are crucial in making informed decisions about reconstructing or repairing building structures. The SonReb method, a combination of the rebound hammer (RH) and the ultrasonic pulse velocity (UPV) tests, is widely used for this purpose. To evaluate the compressive strength, CS, of the concrete under investigation, the ultrasonic pulse velocity Vp and the rebound index R must be mapped to the compressive strength CS using a suitable conversion model, the identification of which requires supplementing the NDT measurements with destructive-type measurements (DT) on a relatively large number of concrete cores. An approach notably indicated in all cases where the minimization of the number of cores is essential is to employ a pre-existing conversion model, i.e., a model derived from previous studies conducted in the literature, which must be appropriately calibrated. In this paper, we investigate the performance of Gaussian process regression (GPR) in calibrating the pre-existing SonReb conversion models, exploiting their ability to handle nonlinearity and uncertainties. The numerical results obtained using experimental data collected from the literature show that GPR calibration is very effective, outperforming, in most cases, the standard multiplicative and additive techniques used to calibrate the SonReb models. Full article
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16 pages, 9163 KiB  
Article
Automated Characterization of the Ply Stacking Sequence of a Woven Carbon Fiber Composite Using Pulse-Echo Ultrasound
by Nathaniel J. Blackman and David A. Jack
J. Compos. Sci. 2023, 7(9), 398; https://doi.org/10.3390/jcs7090398 - 20 Sep 2023
Cited by 6 | Viewed by 1674
Abstract
Carbon fiber composites are a popular design material due to their high specific strength. The directional strength of woven composites can be customized by changing the orientation and sequencing of individual lamina within the ply stack. This allows for the potential of specialized [...] Read more.
Carbon fiber composites are a popular design material due to their high specific strength. The directional strength of woven composites can be customized by changing the orientation and sequencing of individual lamina within the ply stack. This allows for the potential of specialized parts designed for specific applications, leading to both performance gains and weight savings. One challenge is the ability to characterize non-destructively the orientations of the individual lamina after the manufacturing process. Current industrial methods used to verify the ply stack are destructive to the part, increasing costs and material waste. This creates the need for a non-destructive technique capable of determining the ply stack, both for quality control and for in-service parts, including when there may be access to just a single side of the composite. This research introduces a procedure to scan a fabricated laminated composite using pulse-echo ultrasound coupled with an automated algorithm to determine the layer-by-layer orientation of the ply stack with a specific focus on woven composites. In this work, 12 unique plain-weave laminates ranging from 3 lamina to 18 lamina thick are studied. The orientations of each stacking sequence are different, with some following standard composite design methodologies and others randomly stacked. The mathematical technique presented in this work correctly characterizes non-destructively the orientation of each individual lamina to within 1° with 73% confidence and to within 3° with 98.3% confidence of the as-manufactured orientation. Full article
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12 pages, 2652 KiB  
Article
Capillary Rise: A Simple Tool for Simultaneous Determination of Porosity and Thickness of Thin Silica Coatings
by Emmanuel E. Ubuo, Inimfon A. Udoetok, Andrew T. Tyouwa, Clement O. Obadimu and Hamza S. Al-Shehri
J. Compos. Sci. 2023, 7(6), 259; https://doi.org/10.3390/jcs7060259 - 19 Jun 2023
Viewed by 1580
Abstract
Coating porosity is an important property that supports solid-gas and solid-liquid exchange that can either enhance various science and technological applications or promote damage if not properly controlled. However, non-destructive instrumental techniques for the measurement of porosity on coated walls or surfaces can [...] Read more.
Coating porosity is an important property that supports solid-gas and solid-liquid exchange that can either enhance various science and technological applications or promote damage if not properly controlled. However, non-destructive instrumental techniques for the measurement of porosity on coated walls or surfaces can be quite challenging. Here, a seamless capillary rise technique has been used to determine both the thickness and porosity of a thin silica coating. Uniform coatings were prepared from 5 wt% hydrophobic fumed silica in absolute ethanol and spin-coated at 500–8000 rpm on glass slides. Capillary imbibition of squalane was then controlled into known areas of the resulted hydrophobic nano-porous coatings. The mass of the solid (silica) and the infiltrated oil (squalane) were gravimetrically measured. The porosity of the material was calculated as the percentage fraction of the pore volume while the film thickness was determined as the ratio of the total volume to the area of coverage. Mean values of the porosity and coating thickness calculated from capillary impregnation technique were 86 ± 2% and 3.7 ± 0.2 μm, respectively. The coating thickness obtained was comparable with those revealed by SEM and Dektak profiler measurements. This study highlights the effectiveness of capillary rise as a simple and cost-effective non-destructive technique for assessment of coating thickness and porosity. Full article
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