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Mechanical Behavior of Composite Materials (3rd Edition)

A special issue of Materials (ISSN 1996-1944). This special issue belongs to the section "Advanced Composites".

Deadline for manuscript submissions: 31 October 2025 | Viewed by 5449

Special Issue Editor


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Guest Editor
Department of Materials Science and Metallurgical Engineering, University of Oviedo, Edificio Departamental Este, Campus de Viesques, 33203 Gijón, Spain
Interests: composites; mechanical properties; mechanical tests
Special Issues, Collections and Topics in MDPI journals

Special Issue Information

Dear Colleagues,

After our successful first two volume of the Special Issue “Mechanical Behavior of Composite Materials”, we have decided to create the 3rd volume, in order to collect and publish a series of state-of-art research in mechanical behaviors of composites materials.

The appearance of composite materials was a revolution in the field of materials due to their high mechanical properties and lightness. This opened up important expectations for their use in technological components that required stronger and lighter materials. When we talk about mechanical properties, we also talk about fatigue, fracture and creep, and even the strength of adhesive joints, if one of the adhesives is a composite. Another point of recent importance is the additive manufacturing of composites and the modifications that this new configuration of materials brings to the usual study of mechanical properties. In short, this special issue contains all the contributions that allow us to disseminate a better understanding of this exciting family of materials from the point of view of their mechanical properties.

Prof. Dr. Jaime Viña
Guest Editor

Manuscript Submission Information

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Keywords

  • fracture
  • fatigue: creep
  • tensile
  • compression
  • adhesives joints
  • 3D composites
  • mechanical tests
  • mechanical properties

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Related Special Issues

Published Papers (6 papers)

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Research

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10 pages, 4843 KiB  
Article
Improving the Mechanical Properties and Microstructure of 12 mol% Ceria-Stabilized Tetragonal Zirconia Polycrystal Ceramics with Low-Content Nd2O3
by Zengqing Sun, Xiaoyu Li, Jinxin Xing, Min Gan, Zhiyun Ji and Yong Lyu
Materials 2024, 17(22), 5426; https://doi.org/10.3390/ma17225426 - 6 Nov 2024
Viewed by 424
Abstract
In this study, 12 mol% ceria-stabilized tetragonal zirconia polycrystal ceramics with xNd2O3 (where x equals 0, 0.1, 0.2, 0.3, 0.4, 0.5, and 0.7) were synthesized via the solid-state method, and the effects of Nd2O3 doping amounts on [...] Read more.
In this study, 12 mol% ceria-stabilized tetragonal zirconia polycrystal ceramics with xNd2O3 (where x equals 0, 0.1, 0.2, 0.3, 0.4, 0.5, and 0.7) were synthesized via the solid-state method, and the effects of Nd2O3 doping amounts on the mechanical properties and microstructure were studied. The results show that with an increase in the Nd2O3 doping amount, the grain size of the ceramics was reduced from 2.93 μm to 0.69 μm. The hardness and strength of the ceramics increased significantly, while the fracture toughness decreased. The reduction in fracture toughness was attributed to the reduction in tetragonal grain size, which suppressed the tetragonal–monoclinic phase transformation caused by stress. Additionally, as the content of Nd2O3 increased, the formation of cubic zirconia accelerated, but no second phase was observed. Most importantly, when the doping amount of Nd2O3 reached 0.3 mol%, the comprehensive mechanical characteristics of the ceramics were optimal. This provides a research basis for the preparation of nanoscale 12 mol% ceria-stabilized tetragonal zirconia polycrystal ceramics. Full article
(This article belongs to the Special Issue Mechanical Behavior of Composite Materials (3rd Edition))
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11 pages, 4339 KiB  
Article
The Micromechanical Properties and Surface Roughness of Orthodontic Retainer Wires—An In Vitro Analysis
by Maciej Jedliński, Jolanta Krupa and Joanna Janiszewska-Olszowska
Materials 2024, 17(14), 3431; https://doi.org/10.3390/ma17143431 - 11 Jul 2024
Viewed by 790
Abstract
Background: Despite the large variety of retainer wires available, no studies could be found comparing the micromechanical properties and surface roughness of different retainer wires. Such characteristics affect the survival of the fixed retainer in terms of both fracture resistance and resistance to [...] Read more.
Background: Despite the large variety of retainer wires available, no studies could be found comparing the micromechanical properties and surface roughness of different retainer wires. Such characteristics affect the survival of the fixed retainer in terms of both fracture resistance and resistance to debonding from the tooth. Therefore, the aim of the present study was to examine and compare those characteristics in popular retainer wires. Methods: six different popular orthodontic retainer wires were subjected to instrumental indentation based on the Oliver and Pharr method. The geometric surface structure was analysed using a non-contact profilometer. Results: stainless steel wires had a higher hardness and a higher elastic modulus compared to titanium wires and white gold chain. The titanium wire and the white gold chain showed much more roughness than other wires. Conclusions: stainless steel wires are the most resistant, considering both the shape retention capacity and the ability to resist abrasive wear. The titanium wire showed the lowest hardness and, thus, the highest susceptibility to deformation. Bond-a-braid, Retainium and Orthoflex white gold are more resistant to fracture than other steel wires. Titanium wire and chain retainer wires have more roughness, which is a great advantage in terms of mechanical adhesion to composite materials. Full article
(This article belongs to the Special Issue Mechanical Behavior of Composite Materials (3rd Edition))
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15 pages, 7629 KiB  
Article
Investigating the High-Temperature Bonding Performance of Refractory Castables with Ribbed Stainless-Steel Bars
by Linas Plioplys, Valentin Antonovič, Renata Boris, Andrius Kudžma and Viktor Gribniak
Materials 2024, 17(12), 2916; https://doi.org/10.3390/ma17122916 - 14 Jun 2024
Viewed by 853
Abstract
Refractory materials containing calcium aluminate cement (CAC) are commonly used in the metallurgical and petrochemical industries due to their exceptional mechanical resistance, even at temperatures exceeding 1000 °C, and do not require additional reinforcement. This study seeks to advance this practice by developing [...] Read more.
Refractory materials containing calcium aluminate cement (CAC) are commonly used in the metallurgical and petrochemical industries due to their exceptional mechanical resistance, even at temperatures exceeding 1000 °C, and do not require additional reinforcement. This study seeks to advance this practice by developing ultra-high-performance structures that offer building protection against fire and explosions. Such structures require bar reinforcement to withstand accidental tension stresses, and the bond performance becomes crucial. However, the compressive strength of these materials may not correlate with their bond resistance under high-temperature conditions. This study investigates the bond behavior of ribbed stainless austenitic steel bars in refractory materials typical for structural projects. The analysis considers three chamotte-based compositions, i.e., a conventional castable (CC) with 25 wt% CAC, a medium-cement castable (MCC) with 12 wt% CAC, a low-cement castable (LCC), and a low-cement bauxite-based castable (LCB); the LCC and LCB castables contain 7 wt% CAC. The first three refractory compositions were designed to achieve a cold compressive strength (CCS) of 100 MPa, while the LCB mix proportions were set to reach a CCS of 150 MPa. Mechanical and pull-out tests were conducted after treatment at 400 °C, 600 °C, 800 °C, and 1000 °C; reference specimens were not subjected to additional temperature treatment. This study used X-ray fluorescence (XRF), X-ray diffraction (XRD), and scanning electron microscopy (SEM) methods to capture the material alterations. The test results indicated that the bonding resistance, expressed in terms of the pull-out deformation energy, did not directly correlate with the compressive strength, supporting the research hypothesis. Full article
(This article belongs to the Special Issue Mechanical Behavior of Composite Materials (3rd Edition))
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17 pages, 9740 KiB  
Article
The Influence of Microstructural Arrangement on the Failure Characteristics of 3D-Printed Polymers: Exploring Damage Behaviour in Acrylonitrile Butadiene Styrene
by Sofiane Guessasma and Sofiane Belhabib
Materials 2024, 17(11), 2699; https://doi.org/10.3390/ma17112699 - 3 Jun 2024
Viewed by 806
Abstract
This study investigated how printing conditions influence the fracture behaviour of 3D-printed acrylonitrile butadiene styrene (ABS) under tensile loading. Dog-bone-shaped ABS specimens were produced using the fusion filament fabrication technique, with varying printing angles. Tensile tests were conducted on pre-notched specimens with consistent [...] Read more.
This study investigated how printing conditions influence the fracture behaviour of 3D-printed acrylonitrile butadiene styrene (ABS) under tensile loading. Dog-bone-shaped ABS specimens were produced using the fusion filament fabrication technique, with varying printing angles. Tensile tests were conducted on pre-notched specimens with consistent pre-notch lengths but different orientations. Optical and scanning electron microscopies were employed to analyse crack propagation in the pre-notched specimens. In order to support experimental evidence, finite element computation was implemented to study the damage induced by the microstructural rearrangement of the filaments when subject to tensile loading. The findings revealed the simple linear correlation between the failure properties including elongation at break and maximum stress in relation to the printing angle for different pre-notch lengths. A more progressive damage was found to support the ultimate performance of the studied material. This experiment evidence was used to build a damage model of 3D-printed ABS that accounts for the onset, growth, and damage saturation. This damage modelling is able to capture the failure properties as a function of the printing angle using a sigmoid-like damage function and a modulation of the stiffness within the raster. The numerical results demonstrated that damage pattern develops as a result of the filament arrangement and weak adhesion between adjacent filaments and explains the diffuse damage kinetics observed experimentally. This study concludes with a topological law relating the notch size and orientation to the rupture properties of 3D-printed ABS. This study supports the idea of tailoring the microstructural arrangement to control and mitigate the mechanical instabilities that lead to the failure of 3D-printed polymers. Full article
(This article belongs to the Special Issue Mechanical Behavior of Composite Materials (3rd Edition))
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13 pages, 4575 KiB  
Article
Effect of Rare Earth Elements on Microstructure and Tensile Behavior of Nb-Containing Microalloyed Steels
by Shi Cheng, Tingping Hou, Yihang Zheng, Chaochao Yin and Kaiming Wu
Materials 2024, 17(7), 1701; https://doi.org/10.3390/ma17071701 - 8 Apr 2024
Cited by 1 | Viewed by 1223
Abstract
The present investigation endeavors to explore the influence of rare earth elements on the strength and plasticity characteristics of low-carbon microalloyed steel under tensile loading conditions. The findings from the conducted tensile tests indicate that the incorporation of rare earths leads to a [...] Read more.
The present investigation endeavors to explore the influence of rare earth elements on the strength and plasticity characteristics of low-carbon microalloyed steel under tensile loading conditions. The findings from the conducted tensile tests indicate that the incorporation of rare earths leads to a notable enhancement in the yield strength, ultimate tensile strength, and ductility properties of the steel. A comparative analysis of the microstructures reveals that the presence of rare earths significantly refines and optimizes the microstructure of the microalloyed steel. This optimization is manifested through a reduction in grain size, diminution of inclusion sizes, and a concomitant rise in their number density. Moreover, the addition of rare earths is observed to foster an increase in the volumetric fraction of carbides within the steel matrix. These multifaceted microstructural alterations collectively contribute to a substantial strengthening of the microalloyed steel. Furthermore, it is elucidated that the synergistic interaction between rare earth elements and both carbon (C) and niobium (Nb) in the steel matrix augments the extent of the Lüders strain region during the tensile deformation of specimens. This phenomenon is accompanied by the effective modification of inclusions by the rare earths, which serves to mitigate stress concentrations at the interfaces between the inclusions and the surrounding matrix. This article systematically evaluates the modification mechanism of rare earth microalloying, which provides a basis for broadening the application of rare earth microalloying in microalloyed steel. Full article
(This article belongs to the Special Issue Mechanical Behavior of Composite Materials (3rd Edition))
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Review

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17 pages, 3236 KiB  
Review
Anchorage Research for CFRP Tendons: A Review
by Yalong Li, Taining Shi, Yafeng Qiu, Yuanlin Zhu and Longkang Zhang
Materials 2024, 17(13), 3208; https://doi.org/10.3390/ma17133208 - 1 Jul 2024
Viewed by 948
Abstract
Carbon fiber reinforced polymer (CFRP) tendons are composite materials that offer significant advantages in terms of tensile strength and lightweight properties. They are being increasingly utilized in the construction industry, particularly in bridge cables and building structures. However, due to their relatively poor [...] Read more.
Carbon fiber reinforced polymer (CFRP) tendons are composite materials that offer significant advantages in terms of tensile strength and lightweight properties. They are being increasingly utilized in the construction industry, particularly in bridge cables and building structures. However, due to their relatively poor transverse mechanical properties compared to steel cables, securing these tendons with anchors presents a challenge. This paper reviews the structure and force characteristics of three types of anchors for CFRP tendons—clamping anchorage, bonded anchorage, and composite anchorage—analyzes and summarizes the anchorage characteristics and damage mechanisms of each type of anchorage, and highlights that the optimization of the mechanical properties of the tendons is key to the design and research of anchoring systems. The new composite anchorage offers comprehensive advantages, such as minimal tendon damage at the anchorage section, more uniform stress distribution, and better anchorage performance, despite being more complex in design compared to single-type anchorages. However, there remain challenges and research gaps in testing and validating these anchoring systems under realistic loading and environmental conditions, including impacts, cyclic stresses, humidity, and high temperatures. Future efforts should focus on developing new testing techniques and models to simulate real-world conditions, enabling more accurate assessments of anchorage performance and longevity. By doing so, we can fully harness the mechanical properties of CFRP tendons and further enhance the safety and efficiency of our built environment. Full article
(This article belongs to the Special Issue Mechanical Behavior of Composite Materials (3rd Edition))
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